m-formyl-p-hydroxy-benzyl-2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:m-formyl-p-hydroxy-benzyl-2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside
CAS No.:1448810-93-2
Molecular Formula:C₄₆H₅₈O₂₇S
Molecular Weight:1075.02
Hs Code.:

m-formyl-p-hydroxy-benzyl-2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

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Chemical Property of m-formyl-p-hydroxy-benzyl-2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

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Technology Process of m-formyl-p-hydroxy-benzyl-2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

There total 3 articles about m-formyl-p-hydroxy-benzyl-2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23731-06-8
5-(chloromethyl)salicylaldehyde

: C₃₉H₅₅N₂O₂₅S⁽¹⁺⁾*I^(1-)

: 1448810-93-2
m-formyl-p-hydroxy-benzyl-2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

Guidance literature:: With triethylamine; In acetonitrile; at 20 ℃; for 1h;
DOI:10.1021/jo401148f

Reference yield:

: 76821-26-6
maltotriose peracetate

: 1448810-93-2
m-formyl-p-hydroxy-benzyl-2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: iodine; triethylsilane / dichloromethane / 0.5 h / Reflux

2: acetonitrile / 1 h / 60 °C

3: triethylamine / acetonitrile / 1 h / 20 °C

With triethylsilane; iodine; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1021/jo401148f

Reference yield:

: C₃₈H₅₁IO₂₅

: 1448810-93-2
m-formyl-p-hydroxy-benzyl-2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 1 h / 60 °C

2: triethylamine / acetonitrile / 1 h / 20 °C

With triethylamine; In acetonitrile;
DOI:10.1021/jo401148f