9α-Hydroxy acetylmerulidial

Base Information

• Chemical Name: 9α-Hydroxy acetylmerulidial
• CAS No.: 114838-69-6
• Molecular Formula: C₁₇H₂₂O₅
• Molecular Weight: 306.359
• Mol file: 114838-69-6.mol

Synonyms:9a-(Acetyloxy)merulidial; 9a-Acetoxymerulidial

Chemical Property of 9α-Hydroxy acetylmerulidial

Chemical Property:

• Vapor Pressure: 9.83E-09mmHg at 25°C
• Boiling Point: 417.9°C at 760 mmHg
• Flash Point: 147.5°C
• PSA: 80.67000
• Density: 1.26g/cm³
• LogP: 1.57360

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 9α-Hydroxy acetylmerulidial

There total 2 articles about 9α-Hydroxy acetylmerulidial which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Merulidial (68053-32-7) → 8-O-acetyl-9α-hydroxymerulidial (114838-69-6)

Guidance literature:

Multi-step reaction with 2 steps

1: Al₂O₃, O₂ / ethyl acetate; petroleum ether

2: pyridine

With aluminum oxide; oxygen; In pyridine; ethyl acetate; Petroleum ether;

Reference yield:

acetic anhydride (108-24-7) + 9α-hydroxymerulidial (114924-37-7) → 8-O-acetyl-9α-hydroxymerulidial (114838-69-6)

Guidance literature:

In pyridine;

upstream raw materials:

acetic anhydride

9α-hydroxymerulidial

Merulidial

Refernces