Dimenthyl 5-methyl-1,5-cyclohexenyl phosphate

Base Information

Chemical Name:Dimenthyl 5-methyl-1,5-cyclohexenyl phosphate
CAS No.:161258-07-7
Molecular Formula:C₂₇H₄₇O₄P
Molecular Weight:466.642
Hs Code.:

Synonyms:

Suppliers and Price of Dimenthyl 5-methyl-1,5-cyclohexenyl phosphate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Dimenthyl 5-methyl-1,5-cyclohexenyl phosphate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Dimenthyl 5-methyl-1,5-cyclohexenyl phosphate

There total 2 articles about Dimenthyl 5-methyl-1,5-cyclohexenyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 1193-18-6
3-methylcyclohexen-2-one

: 161344-72-5
Phosphorochloridic acid bis-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester

: 161258-07-7
Dimenthyl 5-methyl-1,5-cyclohexenyl phosphate

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; 1.) -78 deg C, 2 h, 2.) -40 deg C;
DOI:10.1021/jo00105a042

Reference yield:

: 2216-51-5
(-)-menthol

: 161258-07-7
Dimenthyl 5-methyl-1,5-cyclohexenyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / phosphorus oxychloride, Et₃N / benzene / 72 h / Heating

2: 24 percent / LDA / tetrahydrofuran / 1.) -78 deg C, 2 h, 2.) -40 deg C

With triethylamine; lithium diisopropyl amide; trichlorophosphate; In tetrahydrofuran; benzene;
DOI:10.1021/jo00105a042