Technology Process of C23H26O
There total 2 articles about C23H26O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1-tert-butyl-4-hexa-1,3,5-triynyl-benzene;
With
(-)-N-methylephedrine; zinc trifluoromethanesulfonate; triethylamine;
In
toluene;
at 20 ℃;
for 0.333333h;
Inert atmosphere;
cyclohexanecarbaldehyde;
In
toluene;
at 20 ℃;
for 90h;
optical yield given as %ee;
enantioselective reaction;
Inert atmosphere;
DOI:10.1021/jo2008719
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: methanol; potassium carbonate / tetrahydrofuran / 20 °C / Inert atmosphere
2.1: (-)-N-methylephedrine; zinc trifluoromethanesulfonate; triethylamine / toluene / 0.33 h / 20 °C / Inert atmosphere
2.2: 90 h / 20 °C / Inert atmosphere
With
methanol; (-)-N-methylephedrine; zinc trifluoromethanesulfonate; potassium carbonate; triethylamine;
In
tetrahydrofuran; toluene;
DOI:10.1021/jo2008719