2-phenylpyrimidine-4,6-dicarboxaldehyde mono{methyl{6-[1-methyl-2-(pyridin-2-ylmethylene)hydrazino]pyrimidin-4-yl}hydrazone}

Base Information

• Chemical Name: 2-phenylpyrimidine-4,6-dicarboxaldehyde mono{methyl{6-[1-methyl-2-(pyridin-2-ylmethylene)hydrazino]pyrimidin-4-yl}hydrazone}
• CAS No.: 618428-75-4
• Molecular Formula: C₂₄H₂₁N₉O
• Molecular Weight: 451.49
• Mol file: 618428-75-4.mol

Synonyms:

Chemical Property of 2-phenylpyrimidine-4,6-dicarboxaldehyde mono{methyl{6-[1-methyl-2-(pyridin-2-ylmethylene)hydrazino]pyrimidin-4-yl}hydrazone}

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-phenylpyrimidine-4,6-dicarboxaldehyde mono{methyl{6-[1-methyl-2-(pyridin-2-ylmethylene)hydrazino]pyrimidin-4-yl}hydrazone}

There total 3 articles about 2-phenylpyrimidine-4,6-dicarboxaldehyde mono{methyl{6-[1-methyl-2-(pyridin-2-ylmethylene)hydrazino]pyrimidin-4-yl}hydrazone} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

2-phenyl-4,6-pyrimidinedicarboxaldehyde (80109-86-0) + 4-(1-methyl-2-(pyridin-2-ylmethylene)hydrazinyl)-6-(1-methylhydrazineyl)pyrimidine (618428-57-2) → 2-phenylpyrimidine-4,6-dicarboxaldehyde mono{methyl{6-[1-methyl-2-(pyridin-2-ylmethylene)hydrazino]pyrimidin-4-yl}hydrazone} (618428-75-4)

Guidance literature:

In ethanol; at 20 ℃; for 30h;

DOI:10.1002/hlca.200390137

Reference yield:

pyridine-2-carbaldehyde (1121-60-4) → 2-phenylpyrimidine-4,6-dicarboxaldehyde mono{methyl{6-[1-methyl-2-(pyridin-2-ylmethylene)hydrazino]pyrimidin-4-yl}hydrazone} (618428-75-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 55 percent / ethanol / 3 h / 20 °C

2: 42 percent / ethanol / 30 h / 20 °C

In ethanol;

DOI:10.1002/hlca.200390137

Reference yield:

4,6-bis(1-methylhydrazino)pyrimidine (618428-20-9) → 2-phenylpyrimidine-4,6-dicarboxaldehyde mono{methyl{6-[1-methyl-2-(pyridin-2-ylmethylene)hydrazino]pyrimidin-4-yl}hydrazone} (618428-75-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 55 percent / ethanol / 3 h / 20 °C

2: 42 percent / ethanol / 30 h / 20 °C

In ethanol;

DOI:10.1002/hlca.200390137

upstream raw materials:

2-phenyl-4,6-pyrimidinedicarboxaldehyde

4-(1-methyl-2-(pyridin-2-ylmethylene)hydrazinyl)-6-(1-methylhydrazineyl)pyrimidine

pyridine-2-carbaldehyde

4,6-bis(1-methylhydrazino)pyrimidine