Octyl(diphenyl)sulfanylidene-lambda~5~-phosphane

Base Information

Chemical Name:Octyl(diphenyl)sulfanylidene-lambda~5~-phosphane
CAS No.:114768-15-9
Molecular Formula:C20H27PS
Molecular Weight:330.474
Hs Code.:
DSSTox Substance ID:DTXSID20569043
Nikkaji Number:J2.664.107A
Wikidata:Q82455742
Mol file:114768-15-9.mol

Synonyms:114768-15-9;Octyl(diphenyl)sulfanylidene-lambda~5~-phosphane;DTXSID20569043

Suppliers and Price of Octyl(diphenyl)sulfanylidene-lambda~5~-phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Octyl(diphenyl)sulfanylidene-lambda~5~-phosphane

Chemical Property:

XLogP3:7.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:9
Exact Mass:330.15710903
Heavy Atom Count:22
Complexity:305

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCCP(=S)(C1=CC=CC=C1)C2=CC=CC=C2

Technology Process of Octyl(diphenyl)sulfanylidene-lambda~5~-phosphane

There total 4 articles about Octyl(diphenyl)sulfanylidene-lambda~5~-phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 111-83-1
1-bromo-octane

: 6591-07-7
diphenylphosphane sulfide

: 114768-15-9
octyl(diphenyl)phosphane sulfide

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; at 20 ℃; for 3h;

Reference yield: 45.0%

: 111-66-0,25068-25-1
oct-1-ene

: 829-85-6
diphenylphosphane

: octan-2-yldiphenylphosphine sulfide

: 114768-15-9
octyl(diphenyl)phosphane sulfide

Guidance literature:: With sulfur; In neat (no solvent); at 70 ℃; regioselective reaction; Green chemistry;
DOI:10.1039/c6gc00903d

Reference yield:

: 829-85-6
diphenylphosphane

: 114768-15-9
octyl(diphenyl)phosphane sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / sulfur / toluene

2: 64 percent / Et₃B; O₂ / dioxane; hexane / 20 °C

With triethyl borane; oxygen; sulfur; In 1,4-dioxane; hexane; toluene;
DOI:10.1055/s-2005-921888