N-(Carbamoylmethyl)-9,10-dihydro-1,9-dimethyl-3,5,7-triphenyl-1H-1,3,2λ⁵,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ⁵-triazaphosphol)-10-amin-5-oxid

Base Information

• Chemical Name: N-(Carbamoylmethyl)-9,10-dihydro-1,9-dimethyl-3,5,7-triphenyl-1H-1,3,2λ⁵,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ⁵-triazaphosphol)-10-amin-5-oxid
• CAS No.: 86213-81-2
• Molecular Formula: C₂₄H₂₆N₈O₂P₂
• Molecular Weight: 520.47

Synonyms:

Chemical Property of N-(Carbamoylmethyl)-9,10-dihydro-1,9-dimethyl-3,5,7-triphenyl-1H-1,3,2λ⁵,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ⁵-triazaphosphol)-10-amin-5-oxid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(Carbamoylmethyl)-9,10-dihydro-1,9-dimethyl-3,5,7-triphenyl-1H-1,3,2λ⁵,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ⁵-triazaphosphol)-10-amin-5-oxid

There total 7 articles about N-(Carbamoylmethyl)-9,10-dihydro-1,9-dimethyl-3,5,7-triphenyl-1H-1,3,2λ⁵,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ⁵-triazaphosphol)-10-amin-5-oxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

glycinamide hydrochloride (1668-10-6) + 10-Chlor-9,10-dihydro-1,9-dimethyl-3,5,7-triphenyl-1H-1,3,2λ5,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ5-triazaphosphol)-5-oxid (86213-73-2,86259-16-7) → N-(Carbamoylmethyl)-9,10-dihydro-1,9-dimethyl-3,5,7-triphenyl-1H-1,3,2λ5,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ5-triazaphosphol)-10-amin-5-oxid (86213-81-2)

Guidance literature:

With triethylamine; In benzene; at 60 ℃; for 3h;

Reference yield:

5,5,10,10-tetrachloro-1,6-dimethyl-3,8-diphenyl-1,5,6,10-tetrahydro-5λ5,10λ5-[1,3,2,4]diazadiphospheto[2,1-c;4,3-c']bis[1,2,4,3]triazaphosphole (63148-50-5) → N-(Carbamoylmethyl)-9,10-dihydro-1,9-dimethyl-3,5,7-triphenyl-1H-1,3,2λ5,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ5-triazaphosphol)-10-amin-5-oxid (86213-81-2)

Guidance literature:

Multi-step reaction with 4 steps

1: 87 percent / CH₂Cl₂ / 12 h / Ambient temperature

2: 93 percent / Et₃N / benzene / 12 h

3: 88 percent / Et₃N / benzene

4: Et₃N / benzene / 3 h / 60 °C

With triethylamine; In dichloromethane; benzene;

Reference yield:

N1-methylbenzamidrazone hydrochloride (28705-52-4) → N-(Carbamoylmethyl)-9,10-dihydro-1,9-dimethyl-3,5,7-triphenyl-1H-1,3,2λ5,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ5-triazaphosphol)-10-amin-5-oxid (86213-81-2)

Guidance literature:

Multi-step reaction with 4 steps

1: 87 percent / CH₂Cl₂ / 12 h / Ambient temperature

2: 93 percent / Et₃N / benzene / 12 h

3: 88 percent / Et₃N / benzene

4: Et₃N / benzene / 3 h / 60 °C

With triethylamine; In dichloromethane; benzene;

upstream raw materials:

glycinamide hydrochloride

10-Chlor-9,10-dihydro-1,9-dimethyl-3,5,7-triphenyl-1H-1,3,2λ⁵,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ⁵-triazaphosphol)-5-oxid

5,5,10,10-tetrachloro-1,6-dimethyl-3,8-diphenyl-1,5,6,10-tetrahydro-5λ⁵,10λ⁵-[1,3,2,4]diazadiphospheto[2,1-c;4,3-c']bis[1,2,4,3]triazaphosphole

P,P-dichlorophenylphosphine oxide

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