Technology Process of O-trimethylsilyl 3,5-dibenzyloxy-4-methoxybenzaldehyde cyanohydrin
There total 6 articles about O-trimethylsilyl 3,5-dibenzyloxy-4-methoxybenzaldehyde cyanohydrin which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
zinc(II) iodide;
In
benzene;
for 24h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.) potassium carbonate, dimethylsilyl dichloride / 1.) DMF, RT, 1 d, 2.) DMF, 2 d
2: 87 percent / potassium carbonate / dimethylformamide / 48 h
3: 90 percent / hydrazinum hydroxide / acetone / 18 h / Heating
4: 93 percent / pyridine / 0 - 20 °C
5: 64 percent / sodium carbonate / ethane-1,2-diol / 75 h / 160 °C
6: 70 percent / zinc iodide / benzene / 24 h
With
pyridine; sodium carbonate; potassium carbonate; hydrazine hydrate; dimethylsilicon dichloride; zinc(II) iodide;
In
ethylene glycol; N,N-dimethyl-formamide; acetone; benzene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 87 percent / potassium carbonate / dimethylformamide / 48 h
2: 90 percent / hydrazinum hydroxide / acetone / 18 h / Heating
3: 93 percent / pyridine / 0 - 20 °C
4: 64 percent / sodium carbonate / ethane-1,2-diol / 75 h / 160 °C
5: 70 percent / zinc iodide / benzene / 24 h
With
pyridine; sodium carbonate; potassium carbonate; hydrazine hydrate; zinc(II) iodide;
In
ethylene glycol; N,N-dimethyl-formamide; acetone; benzene;
