(1R,1'R,6S,6'S)-<16,16,16,16,',16',16'-²H6>-γ,γ-carotin

Base Information

Chemical Name:(1R,1'R,6S,6'S)-<16,16,16,16,',16',16'-²H6>-γ,γ-carotin
CAS No.:79981-72-9
Molecular Formula:C₄₀H₅₆
Molecular Weight:542.837
Hs Code.:

(1R,1'R,6S,6'S)-<16,16,16,16,',16',16'-<sup>2</sup>H6>-γ,γ-carotin

Synonyms:

Suppliers and Price of (1R,1'R,6S,6'S)-<16,16,16,16,',16',16'-²H6>-γ,γ-carotin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,1'R,6S,6'S)-<16,16,16,16,',16',16'-²H6>-γ,γ-carotin

Chemical Property:

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Technology Process of (1R,1'R,6S,6'S)-<16,16,16,16,',16',16'-²H6>-γ,γ-carotin

There total 9 articles about (1R,1'R,6S,6'S)-<16,16,16,16,',16',16'-²H6>-γ,γ-carotin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (3E,7E)-2,9-Diethoxy-3,8-dimethyl-deca-1,3,7,9-tetraen-5-yne

: 79981-72-9
(1R,1'R,6S,6'S)-<16,16,16,16,',16',16'-²H6>-γ,γ-carotin

Guidance literature:: Multi-step reaction with 4 steps

1: 16 percent / ZnCl₂, HOAc / benzene; H₂O / 5 h / 95 °C

2: LiAlH₄ / diethyl ether / 0.17 h / -80 °C

3: 1.) 48percent HBr, 2.) NaHCO₃ / 1.) CH₂Cl₂, -50 - -60 degC, 2.5 min, 2.) ether, r.t.

4: 1.) H₂, chinolin / 1.) Lindar-katalysator / 1.) ethyl acetate, 1.5 h, 2.) heptan, reflux, 1.5 h, irradiation

With quinoline; lithium aluminium tetrahydride; hydrogen bromide; hydrogen; sodium hydrogencarbonate; acetic acid; zinc(II) chloride; Lindlar's catalyst; In diethyl ether; water; benzene;
DOI:10.1002/hlca.19810640504

Reference yield:

: 79936-96-2
2-methyl-4<(1'S,2'R)-2'-methyl-6'-methyliden-2'-trideuteriomethyl-2'-cyclohexyl>-(E)-2-buten-1-al

: 79981-72-9
(1R,1'R,6S,6'S)-<16,16,16,16,',16',16'-²H6>-γ,γ-carotin

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / p-toluenesulfonic acid / ethanol / 96 h

2: 16 percent / ZnCl₂, HOAc / benzene; H₂O / 5 h / 95 °C

3: LiAlH₄ / diethyl ether / 0.17 h / -80 °C

4: 1.) 48percent HBr, 2.) NaHCO₃ / 1.) CH₂Cl₂, -50 - -60 degC, 2.5 min, 2.) ether, r.t.

5: 1.) H₂, chinolin / 1.) Lindar-katalysator / 1.) ethyl acetate, 1.5 h, 2.) heptan, reflux, 1.5 h, irradiation

With quinoline; lithium aluminium tetrahydride; hydrogen bromide; hydrogen; sodium hydrogencarbonate; toluene-4-sulfonic acid; acetic acid; zinc(II) chloride; Lindlar's catalyst; In diethyl ether; ethanol; water; benzene;
DOI:10.1002/hlca.19810640504

Reference yield:

: 79936-98-4
2-methyl-4<(1'S,2'R)-2'-methyl-6'-methyliden-2'-trideuteriomethyl-2'-cyclohexyl>-(E)-2-buten-1-al-diethylacetat

: 79981-72-9
(1R,1'R,6S,6'S)-<16,16,16,16,',16',16'-²H6>-γ,γ-carotin

Guidance literature:: Multi-step reaction with 4 steps

1: 16 percent / ZnCl₂, HOAc / benzene; H₂O / 5 h / 95 °C

2: LiAlH₄ / diethyl ether / 0.17 h / -80 °C

3: 1.) 48percent HBr, 2.) NaHCO₃ / 1.) CH₂Cl₂, -50 - -60 degC, 2.5 min, 2.) ether, r.t.

4: 1.) H₂, chinolin / 1.) Lindar-katalysator / 1.) ethyl acetate, 1.5 h, 2.) heptan, reflux, 1.5 h, irradiation

With quinoline; lithium aluminium tetrahydride; hydrogen bromide; hydrogen; sodium hydrogencarbonate; acetic acid; zinc(II) chloride; Lindlar's catalyst; In diethyl ether; water; benzene;
DOI:10.1002/hlca.19810640504