Technology Process of C26H29N3O5S
There total 6 articles about C26H29N3O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Hoveyda-Grubbs catalyst first generation;
In
1,2-dichloro-ethane;
at 80 ℃;
for 15h;
DOI:10.1016/j.bmcl.2012.03.097
- Guidance literature:
-
Multi-step reaction with 7 steps
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate; lithium chloride / ethanol; toluene / 3.5 h / 80 °C
2: sodium hydride / N,N-dimethyl-formamide / 0 °C
3: water; lithium hydroxide / tetrahydrofuran; methanol / 15 h / 0 °C
4: HATU / N,N-dimethyl-formamide / 6 h / 20 °C
5: water; sodium hydroxide / tetrahydrofuran; methanol / 24 h / 20 °C
6: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide
7: Hoveyda-Grubbs catalyst first generation / 1,2-dichloro-ethane / 15 h / 80 °C
With
tetrakis(triphenylphosphine) palladium(0); Hoveyda-Grubbs catalyst first generation; water; sodium hydride; sodium carbonate; N-ethyl-N,N-diisopropylamine; HATU; lithium chloride; sodium hydroxide; lithium hydroxide;
In
tetrahydrofuran; methanol; ethanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene;
1: Suzuki-Miyaura reaction;
DOI:10.1016/j.bmcl.2012.03.097
- Guidance literature:
-
Multi-step reaction with 4 steps
1: HATU / N,N-dimethyl-formamide / 6 h / 20 °C
2: water; sodium hydroxide / tetrahydrofuran; methanol / 24 h / 20 °C
3: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide
4: Hoveyda-Grubbs catalyst first generation / 1,2-dichloro-ethane / 15 h / 80 °C
With
Hoveyda-Grubbs catalyst first generation; water; N-ethyl-N,N-diisopropylamine; HATU; sodium hydroxide;
In
tetrahydrofuran; methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.03.097