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C26H29N3O5S

Base Information
  • Chemical Name:C26H29N3O5S
  • CAS No.:1384352-40-2
  • Molecular Formula:C26H29N3O5S
  • Molecular Weight:495.599
  • Hs Code.:
C<sub>26</sub>H<sub>29</sub>N<sub>3</sub>O<sub>5</sub>S

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Chemical Property of C26H29N3O5S
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Technology Process of C26H29N3O5S

There total 6 articles about C26H29N3O5S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With Hoveyda-Grubbs catalyst first generation; In 1,2-dichloro-ethane; at 80 ℃; for 15h;
DOI:10.1016/j.bmcl.2012.03.097
Guidance literature:
Multi-step reaction with 7 steps
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate; lithium chloride / ethanol; toluene / 3.5 h / 80 °C
2: sodium hydride / N,N-dimethyl-formamide / 0 °C
3: water; lithium hydroxide / tetrahydrofuran; methanol / 15 h / 0 °C
4: HATU / N,N-dimethyl-formamide / 6 h / 20 °C
5: water; sodium hydroxide / tetrahydrofuran; methanol / 24 h / 20 °C
6: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide
7: Hoveyda-Grubbs catalyst first generation / 1,2-dichloro-ethane / 15 h / 80 °C
With tetrakis(triphenylphosphine) palladium(0); Hoveyda-Grubbs catalyst first generation; water; sodium hydride; sodium carbonate; N-ethyl-N,N-diisopropylamine; HATU; lithium chloride; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; 1: Suzuki-Miyaura reaction;
DOI:10.1016/j.bmcl.2012.03.097
Guidance literature:
Multi-step reaction with 4 steps
1: HATU / N,N-dimethyl-formamide / 6 h / 20 °C
2: water; sodium hydroxide / tetrahydrofuran; methanol / 24 h / 20 °C
3: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide
4: Hoveyda-Grubbs catalyst first generation / 1,2-dichloro-ethane / 15 h / 80 °C
With Hoveyda-Grubbs catalyst first generation; water; N-ethyl-N,N-diisopropylamine; HATU; sodium hydroxide; In tetrahydrofuran; methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.03.097
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