(C₅H₅)2Fe₂(S₂)(SCH₂C₆H₅)2

Base Information

Chemical Name:(C₅H₅)2Fe₂(S₂)(SCH₂C₆H₅)2
CAS No.:62029-06-5
Molecular Formula:C₂₄H₂₄Fe₂S₄
Molecular Weight:552.413
Hs Code.:

(C<sub>5</sub>H<sub>5</sub>)2Fe<sub>2</sub>(S<sub>2</sub>)(SCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)2

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Chemical Property of (C₅H₅)2Fe₂(S₂)(SCH₂C₆H₅)2

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Technology Process of (C₅H₅)2Fe₂(S₂)(SCH₂C₆H₅)2

There total 2 articles about (C₅H₅)2Fe₂(S₂)(SCH₂C₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1313-82-2
sodium sulfide

: 77589-76-5
(C₅H₅Fe(NCCH₃)SCH₂C₆H₅)2⁽²⁺⁾*2PF₆^(1-)

: 62029-06-5
(C₅H₅)2Fe₂(S₂)(SCH₂C₆H₅)2

Guidance literature:: In methanol; water; A mixt. of aq. Na2S in MeOH was added dropwise to a stirred soln. of complex in CH3CN, stirred for 30 min (N2 atm.);; evapd., ppt. was extd. with CS2, filtered, chromd. on alumina wiht benzene;;
DOI:10.1021/ic50222a056

Reference yield:

: 10544-50-0
sulfur

: 52346-17-5
(C₅H₅Fe(CO)SCH₂C₆H₅)2

: {Fe4(η5-C5H5)4S4}

: 77589-78-7
(C₅H₅)4Fe₄S₅

: 62029-06-5
(C₅H₅)2Fe₂(S₂)(SCH₂C₆H₅)2

: 72256-41-8
(C₅H₅)4Fe₄S₆

Guidance literature:: In methyl cyclohexane; A stirred mixt. of complex in methylcyclohexane refluxed with S8 for 3.5 h, cooled to about 40°C (N2 atm.);; chromd. on alumina column with benzene, evapd., ppt. was dissolved in CS2, filtered, EtOH was added, reduced in vol. ppt. was washed with hexane and air-dried;;
DOI:10.1021/ic50222a056