C₂₇H₃₂O₉Se

Base Information

Chemical Name:C₂₇H₃₂O₉Se
CAS No.:130819-53-3
Molecular Formula:C₂₇H₃₂O₉Se
Molecular Weight:579.506
Hs Code.:

C<sub>27</sub>H<sub>32</sub>O<sub>9</sub>Se

Synonyms:

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Chemical Property of C₂₇H₃₂O₉Se

Chemical Property:

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Technology Process of C₂₇H₃₂O₉Se

There total 18 articles about C₂₇H₃₂O₉Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 5707-04-0
Phenylselenyl chloride

: 130819-52-2
C₂₁H₂₈O₉

: 130819-53-3,130847-76-6
C₂₇H₃₂O₉Se

Guidance literature:: With pyridinium p-toluenesulfonate; In ethyl acetate; for 48h; Ambient temperature;
DOI:10.1039/C39900001200

Reference yield:

: 130819-41-9
C₁₇H₂₆O₅

: 130819-53-3,130847-76-6
C₂₇H₃₂O₉Se

Guidance literature:: Multi-step reaction with 17 steps

1: Et₃N / toluene / 24 h / 110 °C

2: 2,6-lutidine / CH₂Cl₂ / 0.5 h / Ambient temperature

3: 88 percent / NaIO₄ / OsO₄ / diethyl ether; H₂O / 18 h / Ambient temperature

4: H₅IO₆ / diethyl ether / 0.08 h / Ambient temperature

5: NaOMe / methanol / 0.5 h / Heating

6: pyridinium toluene-p-sulphonate (PPTS) / 12 h / Ambient temperature

7: tetrahydrofuran; hexane / 18 h / Heating

8: ethane-1,2-diol, pyridinium toluene-p-sulphonate (PPTS) / CH₂Cl₂ / 18 h / Heating

9: 81 percent / chromium trioxide, 3,5-dimethylpyrazole / CH₂Cl₂ / 1 h / Ambient temperature

10: 1.) KN(SiMe₃)2, 2.) 2-p-tolylsulphonyl-3-(p-nitrophenyl)oxaziridine / 1.) toluene, THF, 0 deg C, 1 h, 2.) from -78 deg C to RT

11: NaBH₄ / methanol / 0.5 h / 0 °C

12: 90 percent / pyridinium toluene-p-sulphonate (PPTS) / methanol / 48 h / Ambient temperature

13: 50 percent / m-chloroperbenzoic acid (MCPBA), Na₂HPO₄ / CH₂Cl₂ / 48 h / Ambient temperature

14: pyridine / diethyl ether

15: Bu₄NF*3H₂O / tetrahydrofuran / 48 h / Ambient temperature

16: pyridine

17: 85 percent / pyridinium toluene-p-sulphonate (PPTS) / ethyl acetate / 48 h / Ambient temperature

With pyridine; 2,6-dimethylpyridine; 3,5-dimethyl-1H-pyrazole; chromium(VI) oxide; sodium tetrahydroborate; sodium periodate; disodium hydrogenphosphate; tetrabutyl ammonium fluoride; sodium methylate; pyridinium p-toluenesulfonate; potassium hexamethylsilazane; ethylene glycol; 3-(4-nitrophenyl)-2-p-tolylsulfonyloxaziridine; periodic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; osmium(VIII) oxide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; ethyl acetate; toluene;
DOI:10.1039/C39900001200

Reference yield:

: 130819-43-1,130856-99-4
C₂₃H₄₀O₅Si

: 130819-53-3,130847-76-6
C₂₇H₃₂O₉Se

Guidance literature:: Multi-step reaction with 15 steps

1: 88 percent / NaIO₄ / OsO₄ / diethyl ether; H₂O / 18 h / Ambient temperature

2: H₅IO₆ / diethyl ether / 0.08 h / Ambient temperature

3: NaOMe / methanol / 0.5 h / Heating

4: pyridinium toluene-p-sulphonate (PPTS) / 12 h / Ambient temperature

5: tetrahydrofuran; hexane / 18 h / Heating

6: ethane-1,2-diol, pyridinium toluene-p-sulphonate (PPTS) / CH₂Cl₂ / 18 h / Heating

7: 81 percent / chromium trioxide, 3,5-dimethylpyrazole / CH₂Cl₂ / 1 h / Ambient temperature

8: 1.) KN(SiMe₃)2, 2.) 2-p-tolylsulphonyl-3-(p-nitrophenyl)oxaziridine / 1.) toluene, THF, 0 deg C, 1 h, 2.) from -78 deg C to RT

9: NaBH₄ / methanol / 0.5 h / 0 °C

10: 90 percent / pyridinium toluene-p-sulphonate (PPTS) / methanol / 48 h / Ambient temperature

11: 50 percent / m-chloroperbenzoic acid (MCPBA), Na₂HPO₄ / CH₂Cl₂ / 48 h / Ambient temperature

12: pyridine / diethyl ether

13: Bu₄NF*3H₂O / tetrahydrofuran / 48 h / Ambient temperature

14: pyridine

15: 85 percent / pyridinium toluene-p-sulphonate (PPTS) / ethyl acetate / 48 h / Ambient temperature

With pyridine; 3,5-dimethyl-1H-pyrazole; chromium(VI) oxide; sodium tetrahydroborate; sodium periodate; disodium hydrogenphosphate; tetrabutyl ammonium fluoride; sodium methylate; pyridinium p-toluenesulfonate; potassium hexamethylsilazane; ethylene glycol; 3-(4-nitrophenyl)-2-p-tolylsulfonyloxaziridine; periodic acid; 3-chloro-benzenecarboperoxoic acid; osmium(VIII) oxide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; ethyl acetate;
DOI:10.1039/C39900001200