oct-2-en-2-yl diphenyl phosphate

Base Information

• Chemical Name: oct-2-en-2-yl diphenyl phosphate
• CAS No.: 1253389-94-4
• Molecular Formula: C₂₀H₂₅O₄P
• Molecular Weight: 360.39
• Mol file: 1253389-94-4.mol

Synonyms:

Chemical Property of oct-2-en-2-yl diphenyl phosphate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of oct-2-en-2-yl diphenyl phosphate

There total 2 articles about oct-2-en-2-yl diphenyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

diphenyl hydrogen phosphate (838-85-7) + n-octyne (629-05-0) → oct-2-en-2-yl diphenyl phosphate (1253389-94-4) + oct-2-en-2-yl diphenyl phosphate + oct-1-en-2-yl diphenyl phosphate (87436-98-4)

Guidance literature:

With (triphenylphosphine)gold(I) chloride; silver trifluoromethanesulfonate; In toluene; at 20 ℃; for 9h; optical yield given as %de; regioselective reaction; Inert atmosphere;

DOI:10.1002/anie.201001799

Reference yield:

diphenyl hydrogen phosphate (838-85-7) + n-octyne (629-05-0) → oct-2-en-2-yl diphenyl phosphate (1253389-94-4) + oct-2-en-2-yl diphenyl phosphate

Guidance literature:

With chloro[tris(2,3,4,5,6-pentafluorophenylphosphine)]gold(I); silver trifluoromethanesulfonate; In toluene; at 20 ℃; for 24h; optical yield given as %de; regioselective reaction; Inert atmosphere;

DOI:10.1002/anie.201001799

upstream raw materials:

diphenyl hydrogen phosphate

n-octyne