N-chloroacetamidomethyl-1 dimethoxy-5,8 isoquinoleine

Base Information

Chemical Name:N-chloroacetamidomethyl-1 dimethoxy-5,8 isoquinoleine
CAS No.:118361-97-0
Molecular Formula:C₁₄H₁₅ClN₂O₃
Molecular Weight:294.738
Hs Code.:

Synonyms:

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Chemical Property of N-chloroacetamidomethyl-1 dimethoxy-5,8 isoquinoleine

Chemical Property:

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Technology Process of N-chloroacetamidomethyl-1 dimethoxy-5,8 isoquinoleine

There total 6 articles about N-chloroacetamidomethyl-1 dimethoxy-5,8 isoquinoleine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.5%

: 118361-94-7
aminomethyl-1 dimethoxy-5,8 isoquinoleine

: 79-04-9
chloroacetyl chloride

: 118361-97-0
N-chloroacetamidomethyl-1 dimethoxy-5,8 isoquinoleine

Guidance literature:: With triethylamine; In dichloromethane; for 3h; Ambient temperature;

Reference yield:

: 3600-86-0
2,5-dimethoxyphenethylamine

: 118361-97-0
N-chloroacetamidomethyl-1 dimethoxy-5,8 isoquinoleine

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / toluene / 1 h / 60 °C

2: 66 percent / POCl₃ / acetonitrile / 1 h, reflux, then 80 deg C

3: 80 percent / 10percent Pd/C / decahydronaphthalene / 6 h / Heating

4: 90 percent / hydrazine hydrate / ethanol / 2 h / Heating

5: 72.5 percent / triethylamine / CH₂Cl₂ / 3 h / Ambient temperature

With hydrazine hydrate; triethylamine; trichlorophosphate; palladium on activated charcoal; In ethanol; dichloromethane; toluene; acetonitrile; decalin;

Reference yield:

: 108536-18-1
β-dimethoxy-2,5 phenyl nitro ethylene

: 118361-97-0
N-chloroacetamidomethyl-1 dimethoxy-5,8 isoquinoleine

Guidance literature:: Multi-step reaction with 6 steps

1: LiAlH₄, H₂SO₄ (d= 1.86) / tetrahydrofuran / 24 h / Ambient temperature

2: triethylamine / toluene / 1 h / 60 °C

3: 66 percent / POCl₃ / acetonitrile / 1 h, reflux, then 80 deg C

4: 80 percent / 10percent Pd/C / decahydronaphthalene / 6 h / Heating

5: 90 percent / hydrazine hydrate / ethanol / 2 h / Heating

6: 72.5 percent / triethylamine / CH₂Cl₂ / 3 h / Ambient temperature

With lithium aluminium tetrahydride; sulfuric acid; hydrazine hydrate; triethylamine; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; toluene; acetonitrile; decalin;