Technology Process of C28(13)CH34O6
There total 8 articles about C28(13)CH34O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C27(13)CH32O6;
With
sodium hydride;
In
tetrahydrofuran;
at 20 ℃;
for 0.5h;
Inert atmosphere;
Cooling;
methyl iodide;
In
tetrahydrofuran;
at 0 ℃;
for 3h;
Inert atmosphere;
DOI:10.2174/157017810791112478
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / Inert atmosphere; Cooling; Reflux
2.1: triethylsilane; trifluoroacetic acid / dichloromethane / -20 - 20 °C / Inert atmosphere
3.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere; Cooling
3.2: 3 h / 0 °C / Inert atmosphere
With
triethylsilane; tetra-(n-butyl)ammonium iodide; sodium hydride; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.2174/157017810791112478
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: perchloric acid / 0 - 40 °C
2.1: water; phosphorus tribromide / 15 - 25 °C
3.1: silver carbonate / dichloromethane / 0.17 h / 20 °C / Inert atmosphere; Darkness; Molecular sieve
3.2: 0.5 h / Inert atmosphere; Darkness; Molecular sieve
4.1: sodium methylate / methanol; dichloromethane / 15 h / 20 °C / Inert atmosphere
4.2: Dowex 50W-8X (H+)
5.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 2 h / 50 °C / 37.5 Torr
6.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / Inert atmosphere; Cooling; Reflux
7.1: triethylsilane; trifluoroacetic acid / dichloromethane / -20 - 20 °C / Inert atmosphere
8.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere; Cooling
8.2: 3 h / 0 °C / Inert atmosphere
With
triethylsilane; perchloric acid; water; sodium methylate; phosphorus tribromide; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid; silver carbonate; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.2174/157017810791112478
