N-t-butoxycarbonyl-tryptophanol

Base Information

Chemical Name:N-t-butoxycarbonyl-tryptophanol
CAS No.:110659-38-6
Molecular Formula:C₁₆H₂₂N₂O₃
Molecular Weight:290.362
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-t-butoxycarbonyl-tryptophanol

Chemical Property:

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Technology Process of N-t-butoxycarbonyl-tryptophanol

There total 12 articles about N-t-butoxycarbonyl-tryptophanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 13139-14-5
Boc-Trp-OH

: 110659-38-6,143259-51-2,82689-19-8
N-t-butoxycarbonyl-tryptophanol

Guidance literature:: Boc-Trp-OH; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at -15 ℃; for 0.25h;

With sodium tetrahydroborate; In tetrahydrofuran; water; at -15 ℃; for 1h;
DOI:10.1128/AAC.01152-16

Reference yield: 100.0%

: 219497-33-3
3-(1-benzyl-1H-indol-3-yl)-2-tert-butoxycarbonylamino-propionic acid methyl ester

: 110659-38-6,143259-51-2,82689-19-8
N-t-butoxycarbonyl-tryptophanol

Guidance literature:: With ammonia; sodium; at -40 ℃; for 0.0166667h;
DOI:10.1039/c5ob01438g

Reference yield: 95.0%

: 141215-69-2,33900-28-6
methyl (2S)-2-{[(tert-butoxy)carbonyl]amino}-3-(1H-indol-3-yl)propanoate

: 110659-38-6,143259-51-2,82689-19-8
N-t-butoxycarbonyl-tryptophanol

Guidance literature:: methyl (2S)-2-{[(tert-butoxy)carbonyl]amino}-3-(1H-indol-3-yl)propanoate; With sodium tetrahydroborate; In ethanol; at 0 - 30 ℃; for 10h;

With ammonium chloride; In ethanol; at 0 - 5 ℃;