Technology Process of C32H44N2O4
There total 15 articles about C32H44N2O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: PhCH2ONa / Heating
2: H2, triethylamine / 10 percent Pd/C / tetrahydrofuran / Ambient temperature
With
hydrogen; triethylamine; sodium phenyl-methanolate;
palladium on activated charcoal;
In
tetrahydrofuran;
- Guidance literature:
-
Multi-step reaction with 13 steps
1: 1.) Na / 1.) ethanol; 2.) ethanol, reflux, 0.5 h
2: H2O, KOH / Heating
3: 94.7 percent / quinoline / 0.33 h / Heating
4: 89.4 percent / cc. H2SO4 / toluene
5: 89.6 percent / B2H6 / tetrahydrofuran
6: 91.2 percent / 48 percent HBr / H2O / 0.5 h / Heating
7: 97 percent / ethanol / 4 h / Heating
8: 98 percent / H2O, KOH / ethanol / Heating
9: SOCl2 / Heating
10: SnCl2 / CH2Cl2; nitromethane / Ambient temperature
11: B2H6 / tetrahydrofuran
12: PhCH2ONa / Heating
13: H2, triethylamine / 10 percent Pd/C / tetrahydrofuran / Ambient temperature
With
quinoline; potassium hydroxide; thionyl chloride; sulfuric acid; water; hydrogen bromide; hydrogen; sodium; triethylamine; sodium phenyl-methanolate; tin(ll) chloride; diborane;
palladium on activated charcoal;
In
tetrahydrofuran; nitromethane; ethanol; dichloromethane; water; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: SnCl2 / CH2Cl2; nitromethane / Ambient temperature
2: B2H6 / tetrahydrofuran
3: PhCH2ONa / Heating
4: H2, triethylamine / 10 percent Pd/C / tetrahydrofuran / Ambient temperature
With
hydrogen; triethylamine; sodium phenyl-methanolate; tin(ll) chloride; diborane;
palladium on activated charcoal;
In
tetrahydrofuran; nitromethane; dichloromethane;