C₂₄H₂₇F₂N₅O₃S

Base Information

Chemical Name:C₂₄H₂₇F₂N₅O₃S
CAS No.:1440422-36-5
Molecular Formula:C₂₄H₂₇F₂N₅O₃S
Molecular Weight:503.573
Hs Code.:

C<sub>24</sub>H<sub>27</sub>F<sub>2</sub>N<sub>5</sub>O<sub>3</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₂₇F₂N₅O₃S

Chemical Property:

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Technology Process of C₂₄H₂₇F₂N₅O₃S

There total 6 articles about C₂₄H₂₇F₂N₅O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1315498-14-6
(R)-1-(1-(trans-4-aminocyclohexyl)-6-(phenylsulfonyl)-1,6-dihydroimidazo[4,5-d]pyrrolo[2,3-b]pyridin-2-yl)ethanol

: 74427-22-8
2,2-difluoroethyl triflate

: 1440422-36-5
C₂₄H₂₇F₂N₅O₃S

Guidance literature:: With triethylamine; In dichloromethane; N,N-dimethyl-formamide; at 23 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jm4004895

Reference yield:

: 1315498-13-5
C₂₇H₃₃N₅O₅S

: 1440422-36-5
C₂₄H₂₇F₂N₅O₃S

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / water / 1 h / 23 °C / Inert atmosphere

2: triethylamine / dichloromethane; N,N-dimethyl-formamide / 16 h / 23 °C / Inert atmosphere

With triethylamine; trifluoroacetic acid; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm4004895

Reference yield:

: 1245649-52-8
1-(benzenesulfonyl)-4-chloro-5-nitro-1H-pyrrolo[2,3-b]pyridine

: 1440422-36-5
C₂₄H₂₇F₂N₅O₃S

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 3 h / Inert atmosphere; Reflux

2.1: iron; ammonium chloride / ethanol; water / 4 h / Inert atmosphere; Reflux

3.1: triethyloxonium tetrafluoroborate / tetrahydrofuran / 2 h / 23 °C / Inert atmosphere

3.2: 2 h / Inert atmosphere; Reflux

4.1: trifluoroacetic acid / water / 1 h / 23 °C / Inert atmosphere

5.1: triethylamine / dichloromethane; N,N-dimethyl-formamide / 16 h / 23 °C / Inert atmosphere

With triethyloxonium tetrafluoroborate; iron; ammonium chloride; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jm4004895