Technology Process of C41H44N6O4S3Si
There total 11 articles about C41H44N6O4S3Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: methanol / 0.33 h / 20 °C / Reflux
2: N-Bromosuccinimide / N,N-dimethyl-formamide / 70 °C
3: cesium fluoride; tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / Inert atmosphere; Reflux
4: boron tribromide / dichloromethane / -78 - 20 °C
5: caesium carbonate / toluene; acetone / Reflux
6: copper
With
N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); boron tribromide; copper; caesium carbonate; cesium fluoride;
In
1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; acetone; toluene;
6: |Huisgen Cycloaddition;
DOI:10.1039/c4cc02179g
- Guidance literature:
-
Multi-step reaction with 5 steps
1: N-Bromosuccinimide / N,N-dimethyl-formamide / 70 °C
2: cesium fluoride; tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / Inert atmosphere; Reflux
3: boron tribromide / dichloromethane / -78 - 20 °C
4: caesium carbonate / toluene; acetone / Reflux
5: copper
With
N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); boron tribromide; copper; caesium carbonate; cesium fluoride;
In
1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; acetone; toluene;
5: |Huisgen Cycloaddition;
DOI:10.1039/c4cc02179g
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 20 °C
2.1: lithium diisopropyl amide / tetrahydrofuran / 0.33 h / -78 °C
2.2: 20 °C
3.1: n-butyllithium / diethyl ether / 1.5 h / -78 °C
3.2: 20 °C
4.1: cesium fluoride; tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / Inert atmosphere; Reflux
5.1: boron tribromide / dichloromethane / -78 - 20 °C
6.1: caesium carbonate / toluene; acetone / Reflux
7.1: copper
With
N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; boron tribromide; copper; caesium carbonate; cesium fluoride; lithium diisopropyl amide;
In
tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetone; toluene;
7.1: |Huisgen Cycloaddition;
DOI:10.1039/c4cc02179g