E,E-<2-(1,3,3-trimethylindoline-2-ilidene)ethylidene>-Z-benzylidene succinic anhydride

Base Information

Chemical Name:E,E-<2-(1,3,3-trimethylindoline-2-ilidene)ethylidene>-Z-benzylidene succinic anhydride
CAS No.:147502-54-3
Molecular Formula:C₂₄H₂₁NO₃
Molecular Weight:371.436
Hs Code.:

Synonyms:

Suppliers and Price of E,E-<2-(1,3,3-trimethylindoline-2-ilidene)ethylidene>-Z-benzylidene succinic anhydride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of E,E-<2-(1,3,3-trimethylindoline-2-ilidene)ethylidene>-Z-benzylidene succinic anhydride

Chemical Property:

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Technology Process of E,E-<2-(1,3,3-trimethylindoline-2-ilidene)ethylidene>-Z-benzylidene succinic anhydride

There total 3 articles about E,E-<2-(1,3,3-trimethylindoline-2-ilidene)ethylidene>-Z-benzylidene succinic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1127303-63-2
2-(1,3,3-trimethylindolenylindene)ethenal

: 147502-54-3
E,E-<2-(1,3,3-trimethylindoline-2-ilidene)ethylidene>-Z-benzylidene succinic anhydride

Guidance literature:: Multi-step reaction with 3 steps

1: potassium tert-butoxide / 2-methyl-propan-2-ol / 0.67 h

2: HCl (g) / 56 h / 20 °C

3: 1.) K, 2.) 10percent ethanolic potassium hydroxide / 1.) tert-butyl ether, tert-butanol, reflux, 40 min, 2.) reflux, 1 h

With hydrogenchloride; potassium hydroxide; potassium tert-butylate; In tert-butyl alcohol;
DOI:10.1007/BF00529478

Reference yield:

: 2-[2-[1,3,3-Trimethyl-1,3-dihydro-indol-(2Z)-ylidene]-eth-(Z)-ylidene]-succinic acid

: 147502-54-3
E,E-<2-(1,3,3-trimethylindoline-2-ilidene)ethylidene>-Z-benzylidene succinic anhydride

Guidance literature:: Multi-step reaction with 2 steps

1: HCl (g) / 56 h / 20 °C

2: 1.) K, 2.) 10percent ethanolic potassium hydroxide / 1.) tert-butyl ether, tert-butanol, reflux, 40 min, 2.) reflux, 1 h

With hydrogenchloride; potassium hydroxide;
DOI:10.1007/BF00529478

Reference yield:

: 100-52-7
benzaldehyde

: 147502-53-2
diethyl <2-(1,3,3-trimethylindoline-2-ilidene)ethylidene> succinate

: 147502-54-3
E,E-<2-(1,3,3-trimethylindoline-2-ilidene)ethylidene>-Z-benzylidene succinic anhydride

Guidance literature:: With potassium hydroxide; Yield given. Multistep reaction; 1.) tert-butyl ether, tert-butanol, reflux, 40 min, 2.) reflux, 1 h;
DOI:10.1007/BF00529478