Mn₃(2,4,6-C₆H₂Me₃)6*toluene

Base Information

Chemical Name:Mn₃(2,4,6-C₆H₂Me₃)6*toluene
CAS No.:165269-52-3
Molecular Formula:C₇H₈*C₅₄H₆₆Mn₃
Molecular Weight:972.073
Hs Code.:

Mn<sub>3</sub>(2,4,6-C<sub>6</sub>H<sub>2</sub>Me<sub>3</sub>)6*toluene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Mn₃(2,4,6-C₆H₂Me₃)6*toluene

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Technology Process of Mn₃(2,4,6-C₆H₂Me₃)6*toluene

There total 2 articles about Mn₃(2,4,6-C₆H₂Me₃)6*toluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.3%

: MnCl₂*1.5THF

: 108-88-3,15644-74-3,16713-13-6
toluene

: 2633-66-1
2-mesitylmagnesium bromide

: 165269-52-3
Mn₃(2,4,6-C₆H₂Me₃)6*toluene

Guidance literature:: In tetrahydrofuran; N2-atmosphere; stirring (room temp., 10 h), refluxing (5 h); pptn. on dioxane addn. (stirring, 10 h), filtering, evapn., recrystn. (toluene); elem. anal.;
DOI:10.1021/om00005a028

Reference yield: 50.0%

: 7773-01-5
manganese(ll) chloride

: 2633-66-1
2-mesitylmagnesium bromide

: 165269-52-3
Mn₃(2,4,6-C₆H₂Me₃)6*toluene

Guidance literature:: In tetrahydrofuran; byproducts: MgBrCl; -30°C; addn. of dioxane (pptn. of Mg halides), evapn. of soln. to dryness, recrystn. (hot toluene);
DOI:10.1039/c39830001128