2-brom-2-phenyl-1-(4-pyridyl)-1-ethanon hydrobromid

Base Information

Chemical Name:2-brom-2-phenyl-1-(4-pyridyl)-1-ethanon hydrobromid
CAS No.:101986-12-3
Molecular Formula:BrH*C₁₃H₁₀BrNO
Molecular Weight:357.044
Hs Code.:

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Chemical Property of 2-brom-2-phenyl-1-(4-pyridyl)-1-ethanon hydrobromid

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Technology Process of 2-brom-2-phenyl-1-(4-pyridyl)-1-ethanon hydrobromid

There total 4 articles about 2-brom-2-phenyl-1-(4-pyridyl)-1-ethanon hydrobromid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1017-24-9
2-phenyl-1-pyridin-4-yl-ethanone

: 101986-12-3
2-brom-2-phenyl-1-(4-pyridyl)-1-ethanon hydrobromid

Guidance literature:: With bromine; In acetic acid; for 2h; Ambient temperature;

Reference yield:

: 100-39-0
benzyl bromide

: 101986-12-3
2-brom-2-phenyl-1-(4-pyridyl)-1-ethanon hydrobromid

Guidance literature:: Multi-step reaction with 3 steps

1: diisopropylamin, n-butyllithium (15 percent) / hexane; tetrahydrofuran / 1 h / -78 °C

2: tetrabutylammoniumfluorid-hydrat / hexane; tetrahydrofuran; CH₂Cl₂ / Ambient temperature; stirring overnight

3: 60 percent / brom / acetic acid / 2 h / Ambient temperature

With n-butyllithium; tetrabutyl ammonium fluoride; bromine; diisopropylamine; In tetrahydrofuran; hexane; dichloromethane; acetic acid;

Reference yield:

: 3-Phenyl-2-pyridin-4-yl-2-trimethylsilanyloxy-propionitrile

: 101986-12-3
2-brom-2-phenyl-1-(4-pyridyl)-1-ethanon hydrobromid

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammoniumfluorid-hydrat / hexane; tetrahydrofuran; CH₂Cl₂ / Ambient temperature; stirring overnight

2: 60 percent / brom / acetic acid / 2 h / Ambient temperature

With tetrabutyl ammonium fluoride; bromine; In tetrahydrofuran; hexane; dichloromethane; acetic acid;