Technology Process of C15H19N3O4
There total 4 articles about C15H19N3O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine; thionyl chloride / dichloromethane
2: caesium carbonate; potassium iodide / N,N-dimethyl-formamide / 20 °C
3: trifluoroacetic acid / dichloromethane
With
pyridine; thionyl chloride; caesium carbonate; trifluoroacetic acid; potassium iodide;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.09.103
- Guidance literature:
-
Multi-step reaction with 4 steps
1: acetic acid; sodium nitrite
2: pyridine; thionyl chloride / dichloromethane
3: caesium carbonate; potassium iodide / N,N-dimethyl-formamide / 20 °C
4: trifluoroacetic acid / dichloromethane
With
pyridine; thionyl chloride; caesium carbonate; acetic acid; trifluoroacetic acid; potassium iodide; sodium nitrite;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.09.103