Diethyl 6,7-dihydrothieno[3,2-c]pyridine-2,5(4H)-dicarboxylate

Base Information

Chemical Name:Diethyl 6,7-dihydrothieno[3,2-c]pyridine-2,5(4H)-dicarboxylate
CAS No.:116119-00-7
Molecular Formula:C13H17NO4S
Molecular Weight:283.348
Hs Code.:2934999090
DSSTox Substance ID:DTXSID20558073
Wikidata:Q82440203
Mol file:116119-00-7.mol

Synonyms:Diethyl 6,7-dihydrothieno[3,2-c]pyridine-2,5(4H)-dicarboxylate;116119-00-7;diethyl 6,7-dihydro-4H-thieno[3,2-c]pyridine-2,5-dicarboxylate;RSHJDGWVQSUSTR-UHFFFAOYSA-N;SCHEMBL976216;DTXSID20558073;AM20120464;Diethyl6,7-dihydrothieno[3,2-c]pyridine-2,5(4H)-dicarboxylate;6,7-Dihydro-4H-thieno[3,2-c]pyridine-2,5-dicarboxylic acid diethyl ester;Thieno[3,2-c]pyridine-2,5(4H)-dicarboxylic acid, 6,7-dihydro-, 2,5-diethyl ester

Suppliers and Price of Diethyl 6,7-dihydrothieno[3,2-c]pyridine-2,5(4H)-dicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Diethyl6,7-dihydrothieno[3,2-c]pyridine-2,5(4H)-dicarboxylate 95+%
5g
$ 372.00

Crysdot
Diethyl6,7-dihydrothieno[3,2-c]pyridine-2,5(4H)-dicarboxylate 95+%
10g
$ 559.00

Crysdot
Diethyl6,7-dihydrothieno[3,2-c]pyridine-2,5(4H)-dicarboxylate 95+%
25g
$ 842.00

Alichem
Diethyl6,7-dihydrothieno[3,2-c]pyridine-2,5(4H)-dicarboxylate
10g
$ 693.68

Alichem
Diethyl6,7-dihydrothieno[3,2-c]pyridine-2,5(4H)-dicarboxylate
5g
$ 483.96

Total 2 raw suppliers

Chemical Property of Diethyl 6,7-dihydrothieno[3,2-c]pyridine-2,5(4H)-dicarboxylate

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:434.809oC at 760 mmHg
PKA:-1.60±0.20(Predicted)
Flash Point:216.765oC
PSA：84.08000
Density:1.257±0.06 g/cm3(Predicted)
LogP:2.37730
Storage Temp.:2-8°C
XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:283.08782920
Heavy Atom Count:19
Complexity:350

Purity/Quality:

99% ^*data from raw suppliers

Diethyl6,7-dihydrothieno[3,2-c]pyridine-2,5(4H)-dicarboxylate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C1=CC2=C(S1)CCN(C2)C(=O)OCC

Technology Process of Diethyl 6,7-dihydrothieno[3,2-c]pyridine-2,5(4H)-dicarboxylate

There total 2 articles about Diethyl 6,7-dihydrothieno[3,2-c]pyridine-2,5(4H)-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-ethoxycarbonylmethylsulfanyl-5-formyl-3,6-dihydro-2H-pyridine-1-carboxylic acid ethyl ester

: 116119-00-7
6,7-Dihydro-4H-thieno[3,2-c]pyridine-2,5-dicarboxylic acid diethyl ester

Guidance literature:: With potassium hydroxide;
DOI:10.1016/S0960-894X(02)00485-7

Reference yield:

: 96507-72-1
ethyl 4-chloro-3-formyl-5,6-dihydropyridine-1(2H)-carboxylate

: 116119-00-7
6,7-Dihydro-4H-thieno[3,2-c]pyridine-2,5-dicarboxylic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N; pyridine

2: 50 percent aq. KOH

With pyridine; potassium hydroxide; triethylamine;
DOI:10.1016/S0960-894X(02)00485-7