[pyridine-2-C(H)=N(C₆H₅)]palladium(II) bis-trifluoroacetate

Base Information

• Chemical Name: [pyridine-2-C(H)=N(C₆H₅)]palladium(II) bis-trifluoroacetate
• CAS No.: 454678-25-2
• Molecular Formula: C₁₆H₁₀F₆N₂O₄Pd
• Molecular Weight: 514.677
• Mol file: 454678-25-2.mol

Synonyms:

Chemical Property of [pyridine-2-C(H)=N(C₆H₅)]palladium(II) bis-trifluoroacetate

Chemical Property:

Purity/Quality:

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Technology Process of [pyridine-2-C(H)=N(C₆H₅)]palladium(II) bis-trifluoroacetate

There total 1 articles about [pyridine-2-C(H)=N(C₆H₅)]palladium(II) bis-trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

2-(phenyliminomethyl)pyridine (7032-25-9) + palladium(II) trifluoroacetate → [pyridine-2-C(H)=N(C6H5)]palladium(II) bis-trifluoroacetate (454678-25-2)

Guidance literature:

In methanol; dichloromethane; diimine ligand dissolved in CH2Cl2 added to a CH3OH soln. of Pd(CF3COO)2under a nitrogen atmosphere using Schlenk-type techniqies, stirred for 10 min; volume reduced under a steady stream of nitrogen, portionsweise additionof diethyl ether, precipitate collected on a sintered-glass frit, washe d with petroleum ether, dried in a stream of nitrogen, elem. anal.;

DOI:10.1039/b108804c

upstream raw materials:

2-(phenyliminomethyl)pyridine