(+/-)-cis,anti-4,5,6,6a,6b,7,8,12b-octahydrobenzofluoranthene

Base Information

• Chemical Name: (+/-)-cis,anti-4,5,6,6a,6b,7,8,12b-octahydrobenzofluoranthene
• CAS No.: 19390-93-3
• Molecular Formula: C₂₀H₂₀
• Molecular Weight: 260.379

Synonyms:

Chemical Property of (+/-)-cis,anti-4,5,6,6a,6b,7,8,12b-octahydrobenzofluoranthene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (+/-)-cis,anti-4,5,6,6a,6b,7,8,12b-octahydrobenzofluoranthene

There total 7 articles about (+/-)-cis,anti-4,5,6,6a,6b,7,8,12b-octahydrobenzofluoranthene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-Dihydronaphthalene (447-53-0) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → tetralin (119-64-2) + 1-phenyl-1,2,3,4-tetrahydronaphthalene (3018-20-0) + (+/-)-cis,syn-4,5,6,6a,6b,7,8,12b,octahydrobenzofluoranthene (74983-82-7) + (+/-)-cis,anti-4,5,6,6a,6b,7,8,12b-octahydrobenzofluoranthene (19390-93-3,23672-05-1,23756-78-7,74983-81-6,74983-82-7)

Guidance literature:

zirconium(IV) oxide; at 130 ℃; for 4h; Further byproducts given;

Reference yield:

1,2-Dihydronaphthalene (447-53-0) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → naphthalene (91-20-3,71998-51-1,72931-45-4) + tetralin (119-64-2) + 1-phenyl-1,2,3,4-tetrahydronaphthalene (3018-20-0) + (+/-)-cis,syn-4,5,6,6a,6b,7,8,12b,octahydrobenzofluoranthene (74983-82-7) + (+/-)-cis,anti-4,5,6,6a,6b,7,8,12b-octahydrobenzofluoranthene (19390-93-3,23672-05-1,23756-78-7,74983-81-6,74983-82-7)

Guidance literature:

zirconium(IV) oxide; at 130 ℃; for 4h; Mechanism;

Reference yield:

tetralin (119-64-2) → naphthalene (91-20-3,71998-51-1,72931-45-4) + 4,5,6,6a,6b,7,8,12b-octahydro-benzo[j]fluoranthene (19390-93-3,23672-05-1,23756-78-7,74983-82-7)

Guidance literature:

With hydrogenchloride; aluminium trichloride; at 35 - 80 ℃;

DOI:10.1021/ja01164a047

upstream raw materials:

tetralin

aluminium trichloride

1,2-Dihydronaphthalene

benzene

Downstream raw materials:

Benzo[j]fluoranthene

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