1-fluoro-2-oxobutylphosphonate de diethyle

Base Information

Chemical Name:1-fluoro-2-oxobutylphosphonate de diethyle
CAS No.:124050-40-4
Molecular Formula:C₈H₁₆FO₄P
Molecular Weight:226.185
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-fluoro-2-oxobutylphosphonate de diethyle

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Technology Process of 1-fluoro-2-oxobutylphosphonate de diethyle

There total 2 articles about 1-fluoro-2-oxobutylphosphonate de diethyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 146036-63-7,124050-38-0
2-(diethoxyphosphinyl)-2-fluoro-acetic acid chloride

: 1067-73-8
diethyl (2-oxobutyl)phosphonate

: 124050-40-4
1-fluoro-2-oxobutylphosphonate de diethyle

Guidance literature:: at -78 - -45 ℃; for 3h;
DOI:10.1016/0040-4039(88)85251-1

Reference yield: 10.0%

: 557-18-6
diethylmagnesium

: 146036-63-7,124050-38-0
2-(diethoxyphosphinyl)-2-fluoro-acetic acid chloride

: 1067-73-8
diethyl (2-oxobutyl)phosphonate

: 124050-40-4
1-fluoro-2-oxobutylphosphonate de diethyle

Guidance literature:: With lithium chloride; copper(I) bromide; In tetrahydrofuran; diethyl ether; 1.) from -78 deg C to -45 deg C; 2.) -45 deg C, 2.5 h;