Ethanesulfonic acid, 2-[[2-amino-3-(4-hydroxyphenyl)-1-oxopropyl]amino]-, (S)-

Base Information

Chemical Name:Ethanesulfonic acid, 2-[[2-amino-3-(4-hydroxyphenyl)-1-oxopropyl]amino]-, (S)-
CAS No.:116394-11-7
Molecular Formula:C₁₁H₁₆N₂O₅S
Molecular Weight:288.324
Hs Code.:
Mol file:116394-11-7.mol

Synonyms:

Suppliers and Price of Ethanesulfonic acid, 2-[[2-amino-3-(4-hydroxyphenyl)-1-oxopropyl]amino]-, (S)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethanesulfonic acid, 2-[[2-amino-3-(4-hydroxyphenyl)-1-oxopropyl]amino]-, (S)-

Chemical Property:

Purity/Quality:

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Technology Process of Ethanesulfonic acid, 2-[[2-amino-3-(4-hydroxyphenyl)-1-oxopropyl]amino]-, (S)-

There total 6 articles about Ethanesulfonic acid, 2-[[2-amino-3-(4-hydroxyphenyl)-1-oxopropyl]amino]-, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23234-32-4
N-Boc-Tyr(Bn)-Gly-OMe

: 116394-11-7
L-tyrosyltaurine

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / LiCl, NaBH₄ / tetrahydrofuran; ethanol / 20 h / Ambient temperature

2: 74 percent / CBr₄, Ph₃P / CH₂Cl₂ / 20 h / Ambient temperature

3: 90 percent / dimethylformamide / 20 h / Ambient temperature

4: HCOOH, 30percent H₂O₂ / 20 h / Ambient temperature

5: H₂, 98percent aq. HCOOH, 30percent H₂O₂ / 10percent Pd/C / 10 h

With sodium tetrahydroborate; formic acid; carbon tetrabromide; hydrogen; dihydrogen peroxide; triphenylphosphine; lithium chloride; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 143799-85-3
(S)-2-((S)-O-benzyl-N-tert-butoxycarbonyltyrosylamino)ethanol

: 116394-11-7
L-tyrosyltaurine

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / CBr₄, Ph₃P / CH₂Cl₂ / 20 h / Ambient temperature

2: 90 percent / dimethylformamide / 20 h / Ambient temperature

3: HCOOH, 30percent H₂O₂ / 20 h / Ambient temperature

4: H₂, 98percent aq. HCOOH, 30percent H₂O₂ / 10percent Pd/C / 10 h

With formic acid; carbon tetrabromide; hydrogen; dihydrogen peroxide; triphenylphosphine; palladium on activated charcoal; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 143799-89-7
(S)-1-bromo-2-((S)-O-benzyl-N-tert-butoxycarbonyltyrosylamino)ethane

: 116394-11-7
L-tyrosyltaurine

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / dimethylformamide / 20 h / Ambient temperature

2: HCOOH, 30percent H₂O₂ / 20 h / Ambient temperature

3: H₂, 98percent aq. HCOOH, 30percent H₂O₂ / 10percent Pd/C / 10 h

With formic acid; hydrogen; dihydrogen peroxide; palladium on activated charcoal; In N,N-dimethyl-formamide;