2-Methoxy-5-methyl-beta-phenylbenzenepropanal

Base Information

Chemical Name:2-Methoxy-5-methyl-beta-phenylbenzenepropanal
CAS No.:857288-55-2
Molecular Formula:C₁₇H₁₈O₂
Molecular Weight:254.329
Hs Code.:
European Community (EC) Number:948-110-6
DSSTox Substance ID:DTXSID101267800

Synonyms:SCHEMBL3963434;DTXSID101267800;857288-55-2

Suppliers and Price of 2-Methoxy-5-methyl-beta-phenylbenzenepropanal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2-Methoxy-5-methyl-beta-phenylbenzenepropanal

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:254.130679813
Heavy Atom Count:19
Complexity:270

Purity/Quality:: 99.9% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC(=C(C=C1)OC)C(CC=O)C2=CC=CC=C2

Technology Process of 2-Methoxy-5-methyl-beta-phenylbenzenepropanal

There total 6 articles about 2-Methoxy-5-methyl-beta-phenylbenzenepropanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [(E)-(S)-3-(2-Methoxy-5-methyl-phenyl)-3-phenyl-propenyloxy]-trimethyl-silane

: 857288-55-2
(S)-3-(2-methoxy-5-methylphenyl)-3-phenylpropanal

Guidance literature:: With potassium carbonate; In methanol; water; at 20 ℃; for 1h;
DOI:10.1016/j.tetasy.2006.01.036

Reference yield:

: 889135-71-1
(E)-3-(2-methoxy-5-methylphenyl)acrylaldehyde

: 857288-55-2
(S)-3-(2-methoxy-5-methylphenyl)-3-phenylpropanal

Guidance literature:: Multi-step reaction with 2 steps

1: chiral binaphthyl-based rhodium complex / tetrahydrofuran / 1 h / 20 °C

2: potassium carbonate / methanol; H₂O / 1 h / 20 °C

With potassium carbonate; chiral binaphthyl-based rhodium; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.tetasy.2006.01.036

Reference yield:

: (E)-3-(2-Methoxy-5-methyl-phenyl)-acryloyl chloride

: 857288-55-2
(S)-3-(2-methoxy-5-methylphenyl)-3-phenylpropanal

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / LiAlH(Ot-Bu)3 / tetrahydrofuran / 1.5 h / -78 - 20 °C

2: chiral binaphthyl-based rhodium complex / tetrahydrofuran / 1 h / 20 °C

3: potassium carbonate / methanol; H₂O / 1 h / 20 °C

With potassium carbonate; lithium tri-t-butoxyaluminum hydride; chiral binaphthyl-based rhodium; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.tetasy.2006.01.036