3,3-bis(trifluoromethyl)-1,1,1-triphenyl-3H-2,1-benzoxastibole

Base Information

Chemical Name:3,3-bis(trifluoromethyl)-1,1,1-triphenyl-3H-2,1-benzoxastibole
CAS No.:119274-12-3
Molecular Formula:C₂₇H₁₉F₆OSb
Molecular Weight:595.188
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3-bis(trifluoromethyl)-1,1,1-triphenyl-3H-2,1-benzoxastibole

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Technology Process of 3,3-bis(trifluoromethyl)-1,1,1-triphenyl-3H-2,1-benzoxastibole

There total 1 articles about 3,3-bis(trifluoromethyl)-1,1,1-triphenyl-3H-2,1-benzoxastibole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 70091-67-7
lithium 1,1,1,3,3,3-hexafluoro-2-(2-lithiophenyl)-2-propoxide

: 20265-30-9
triphenylantimony dibromide

: 119274-12-3
3,3-bis(trifluoromethyl)-1,1,1-triphenyl-3H-2,1-benzoxastibole

Guidance literature:: In tetrahydrofuran; hexane; stirring (N2 atmosphere, 20 h, room temp.), quenching (excess cold H2O); extn. (Et2O), evapn., chromy. (ethyl acetate/hexane), crystn. (C6H6), elem. anal.;
DOI:10.1021/ja00188a049