C₄₇H₈₅N₂O₂⁽¹⁺⁾*I^(1-)

Base Information

Chemical Name:C₄₇H₈₅N₂O₂⁽¹⁺⁾*I^(1-)
CAS No.:1301603-13-3
Molecular Formula:C₄₇H₈₅N₂O₂*I
Molecular Weight:837.109
Hs Code.:

C<sub>47</sub>H<sub>85</sub>N<sub>2</sub>O<sub>2</sub><sup>(1+)</sup>*I<sup>(1-)</sup>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₇H₈₅N₂O₂⁽¹⁺⁾*I^(1-)

Chemical Property:

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Technology Process of C₄₇H₈₅N₂O₂⁽¹⁺⁾*I^(1-)

There total 6 articles about C₄₇H₈₅N₂O₂⁽¹⁺⁾*I^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1301603-26-8
C₄₆H₈₂N₂O₂

: 74-88-4
methyl iodide

: 1301603-13-3
C₄₇H₈₅N₂O₂⁽¹⁺⁾*I^(1-)

Guidance literature:: In tetrahydrofuran; at 20 - 70 ℃; Inert atmosphere; Darkness;
DOI:10.1002/chem.201001921

Reference yield:

: 1141892-79-6
C₁₀H₁₀N₂O₂

: 1301603-13-3
C₄₇H₈₅N₂O₂⁽¹⁺⁾*I^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / butanone / 48 h / Reflux; Inert atmosphere

2: tetrahydrofuran / 20 - 70 °C / Inert atmosphere; Darkness

With potassium carbonate; potassium iodide; In tetrahydrofuran; butanone;
DOI:10.1002/chem.201001921

Reference yield:

: 192988-59-3
2-(3,4-dimethoxyphenyl)-4,5-dihydro-1H-imidazole

: 1301603-13-3
C₄₇H₈₅N₂O₂⁽¹⁺⁾*I^(1-)

Guidance literature:: Multi-step reaction with 5 steps

1.1: [bis(acetoxy)iodo]benzene; potassium carbonate / dimethyl sulfoxide / 24 h / 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 20 - 55 °C / Inert atmosphere

2.2: 3 h / 20 °C

3.1: pyridine hydrochloride / 5 h / 200 °C / Inert atmosphere

4.1: potassium carbonate; potassium iodide / butanone / 48 h / Reflux; Inert atmosphere

5.1: tetrahydrofuran / 20 - 70 °C / Inert atmosphere; Darkness

With [bis(acetoxy)iodo]benzene; pyridine hydrochloride; sodium hydride; potassium carbonate; potassium iodide; In tetrahydrofuran; dimethyl sulfoxide; butanone; mineral oil;
DOI:10.1002/chem.201001921