1,2,3,3a,4,9b-Hexahydro-2,3-diphenyl[1]benzopyrano[4,3-b]pyrrole

Base Information

Chemical Name:1,2,3,3a,4,9b-Hexahydro-2,3-diphenyl[1]benzopyrano[4,3-b]pyrrole
CAS No.:77234-01-6
Molecular Formula:C₂₃H₂₁NO
Molecular Weight:327.426
Hs Code.:
ChEMBL ID:CHEMBL4970268
DSSTox Substance ID:DTXSID601170444

Synonyms:CHEMBL4970268;DTXSID601170444;1,2,3,3a,4,9b-Hexahydro-2,3-diphenyl[1]benzopyrano[4,3-b]pyrrole;77234-01-6

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2,3,3a,4,9b-Hexahydro-2,3-diphenyl[1]benzopyrano[4,3-b]pyrrole

Chemical Property:

XLogP3:4.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:327.162314293
Heavy Atom Count:25
Complexity:439

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1C2C(C(NC2C3=CC=CC=C3O1)C4=CC=CC=C4)C5=CC=CC=C5

Technology Process of 1,2,3,3a,4,9b-Hexahydro-2,3-diphenyl[1]benzopyrano[4,3-b]pyrrole

There total 3 articles about 1,2,3,3a,4,9b-Hexahydro-2,3-diphenyl[1]benzopyrano[4,3-b]pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 77234-11-8
Benzyl-[1-[2-((E)-3-phenyl-allyloxy)-phenyl]-meth-(E)-ylidene]-amine

: 77234-01-6
2,3-diphenylperhydropyrro<3,2-c>benzopyrane

: 77234-02-7,77234-03-8
cis-3-benzylamino-2-styryl-2,3-dihydrobenzofuran

: 77234-02-7,77234-03-8
trans-3-benzylamino-2-styryl-2,3-dihydrobenzofuran

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; 1.) -70 deg C, 2.) -70 deg C - room temperature, 1 h, 3.) room temperature, 2 h;
DOI:10.1246/cl.1981.135

Reference yield:

: 52846-87-4
2-(3-phenylallyloxy)benzaldehyde

: 77234-01-6
2,3-diphenylperhydropyrro<3,2-c>benzopyrane

Guidance literature:: Multi-step reaction with 2 steps

2: 16 percent / butyllithium / tetrahydrofuran; hexane / 1.) -70 deg C, 2.) -70 deg C - room temperature, 1 h, 3.) room temperature, 2 h

With n-butyllithium; In tetrahydrofuran; hexane;
DOI:10.1246/cl.1981.135

Reference yield:

: 100-46-9
benzylamine

: 77234-01-6
2,3-diphenylperhydropyrro<3,2-c>benzopyrane

Guidance literature:: Multi-step reaction with 2 steps

2: 16 percent / butyllithium / tetrahydrofuran; hexane / 1.) -70 deg C, 2.) -70 deg C - room temperature, 1 h, 3.) room temperature, 2 h

With n-butyllithium; In tetrahydrofuran; hexane;
DOI:10.1246/cl.1981.135