[ZrCl3(κ3-N2P-(tert-butyl)NSiMe2N(CH2CH2P(i-Pr)2)2)]

Base Information

Chemical Name:[ZrCl3(κ3-N2P-(tert-butyl)NSiMe2N(CH2CH2P(i-Pr)2)2)]
CAS No.:1001195-98-7
Molecular Formula:C₂₂H₅₁Cl₃N₂P₂SiZr
Molecular Weight:631.276
Hs Code.:

Synonyms:

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Chemical Property of [ZrCl3(κ3-N2P-(tert-butyl)NSiMe2N(CH2CH2P(i-Pr)2)2)]

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Technology Process of [ZrCl3(κ3-N2P-(tert-butyl)NSiMe2N(CH2CH2P(i-Pr)2)2)]

There total 1 articles about [ZrCl3(κ3-N2P-(tert-butyl)NSiMe2N(CH2CH2P(i-Pr)2)2)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1064078-46-1
2,6-bis(2,4,6-trimethylphenyl)phenyl isocyanide

: 1160287-41-1
[ZrCl(κ3-N2P-(tert-butyl)NSiMe2N(CH2CH2P(i-Pr)2)2)]2(μ-Cl)2

: 1001195-98-7
[ZrCl3(κ3-N2P-(tert-butyl)NSiMe2N(CH2CH2P(i-Pr)2)2)]

: 1160287-45-5
[ZrCl((2,6-mesityl)2C6H3NC)(κ3-N2P-(tert-butyl)NSiMe2N(CH2CH2P(i-Pr)2)2)]

Guidance literature:: In benzene-d6; using Schlenk techniques; addn. of 1:1 mixt. of 2,6-Mes3C6H3NC and (ZrCl((t-Bu)NSiMe2N(CH2CH2P(i-Pr)2)2))2(μ-Cl)2 to NMR tube; dissolving in C6D6 at room temp.; monitoring by NMR;
DOI:10.1021/om8011932

Reference yield: 18.0%

: 1064078-46-1
2,6-bis(2,4,6-trimethylphenyl)phenyl isocyanide

: 1001195-98-7
[ZrCl3(κ3-N2P-(tert-butyl)NSiMe2N(CH2CH2P(i-Pr)2)2)]

: 1160287-47-7
[Zr(Me3C13H6NC6H2Me3)(κ3-N2P-(tert-butyl)NSiMe2N(CH2CH2P(i-Pr)2)2)]

Guidance literature:: With KC₈; In diethyl ether; using Schlenk techniques; addn. suspn. of KC8 in Et2O to suspn. of ZrCl3((t-Bu)NSiMe2N(CH2CH2P(i-Pr)2)2) and 2,6-Mes2C6H3NC in Et2O at -40°C; warming to room temp.; stirring overnight; filtration, concn., cooling at -40°C overnight; crystn.; elem. anal.;
DOI:10.1021/om8011932