4-Hydroxy-3-methoxybenzaldehyde 2,4-dinitrophenyl hydrazone

Base Information

• Chemical Name: 4-Hydroxy-3-methoxybenzaldehyde 2,4-dinitrophenyl hydrazone
• CAS No.: 1166-13-8
• Molecular Formula: C14H12N4O6
• Molecular Weight: 332.272
• Mol file: 1166-13-8.mol

Synonyms:Vanillin-2,4-dinitrophenylhydrazon;2-Methoxy-4-(2,4-dinitro-phenylhydrazonomethyl)-phenol;Vanillin-<2,4-dinitro-phenylhydrazon>;<3-Methoxy-4-hydroxy-benzaldehyd>-2.4-dinitro-phenylhydrazon;vanillin-(2,4-dinitro-phenylhydrazone);4-[(2,4-Dinitro-phenyl)-hydrazonomethyl]-2-methoxy-phenol;Vanillin-(2,4-dinitro-phenylhydrazon);

Chemical Property of 4-Hydroxy-3-methoxybenzaldehyde 2,4-dinitrophenyl hydrazone

Chemical Property:

• PSA: 145.49000
• LogP: 3.78260

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Hydroxy-3-methoxybenzaldehyde 2,4-dinitrophenyl hydrazone

There total 1 articles about 4-Hydroxy-3-methoxybenzaldehyde 2,4-dinitrophenyl hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

vanillin (121-33-5,8014-42-4) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → 3-methoxy-4-hydroxybenzaldehyde-2,4-dinitrophenylhydrazone (1166-13-8)

Guidance literature:

With sulfuric acid; In methanol; at 0 - 25 ℃; for 24h;

DOI:10.1155/2020/2720697

upstream raw materials:

vanillin

(2,4-dinitro-phenyl)-hydrazine