[Fc(NH₂)₂]RuCl₂(PPh₃)₂

Base Information

Chemical Name:[Fc(NH₂)₂]RuCl₂(PPh₃)₂
CAS No.:1383970-53-3
Molecular Formula:C₄₆H₄₂Cl₂FeN₂P₂Ru
Molecular Weight:912.623
Hs Code.:

[Fc(NH<sub>2</sub>)<sub>2</sub>]RuCl<sub>2</sub>(PPh<sub>3</sub>)<sub>2</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Fc(NH₂)₂]RuCl₂(PPh₃)₂

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Technology Process of [Fc(NH₂)₂]RuCl₂(PPh₃)₂

There total 1 articles about [Fc(NH₂)₂]RuCl₂(PPh₃)₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 15529-49-4,41756-81-4
tris(triphenylphosphine)ruthenium(II) chloride

: 1,1'-ferrocene diamine

: 1383970-53-3
[1,1'-diaminoferrocene]RuCl₂(PPh₃)2

Guidance literature:: In dichloromethane; byproducts: P(C6H5)3; soln. of diaminoferrocene (1.46 mmol) in CH2Cl2 added dropwise to soln. of Ru compd. (1.46 mmol) in CH2Cl2 under stirring, mixt. stirred overnight; evapn. under vac., solid washed with Et2O, dissolved in CH2Cl2, soln. filtered through Celite, filtrate layered with hexane, stored for 2 d, crystals collected, dried under vac.; elem. anal.;
DOI:10.1039/c2dt31075a

Reference yield: 78.0%

: 1383970-53-3
[1,1'-diaminoferrocene]RuCl₂(PPh₃)2

: 1383970-54-4
[fc(NH)2]Ru(PPh₃)2

Guidance literature:: With KOC(CH₃)3; In tetrahydrofuran; byproducts: KCl, (CH3)3COH; soln. of KOtBu (0.780 mmol) in THF added dropwise to soln. of FeRu compd. (0.390 mmol) in THF at -78°C, mixt. stirred for 1 h, warmed to room temp., stirred for 2 h; evapn. under vac., residue dissolved in toluene, soln. filtered through Celite, filtrate layered with pentane, crystals isolated; elem. anal.;
DOI:10.1039/c2dt31075a