2,8,9-Triazabicyclo[3.3.1]nona-3,6-diene-8,9-dicarboxylic acid, 2-(4-chlorophenyl)-3-phenyl-, bis(2,2,2-trichloroethyl) ester

Base Information

Chemical Name:2,8,9-Triazabicyclo[3.3.1]nona-3,6-diene-8,9-dicarboxylic acid, 2-(4-chlorophenyl)-3-phenyl-, bis(2,2,2-trichloroethyl) ester
CAS No.:116692-94-5
Molecular Formula:C₂₄H₁₈Cl₇N₃O₄
Molecular Weight:660.596
Hs Code.:
Mol file:116692-94-5.mol

Synonyms:

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Chemical Property of 2,8,9-Triazabicyclo[3.3.1]nona-3,6-diene-8,9-dicarboxylic acid, 2-(4-chlorophenyl)-3-phenyl-, bis(2,2,2-trichloroethyl) ester

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MSDS Files:: SDS file from LookChem

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Technology Process of 2,8,9-Triazabicyclo[3.3.1]nona-3,6-diene-8,9-dicarboxylic acid, 2-(4-chlorophenyl)-3-phenyl-, bis(2,2,2-trichloroethyl) ester

There total 2 articles about 2,8,9-Triazabicyclo[3.3.1]nona-3,6-diene-8,9-dicarboxylic acid, 2-(4-chlorophenyl)-3-phenyl-, bis(2,2,2-trichloroethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109853-26-1
2-hydroxy-4-phenacyl-1,2,3,4-tetrahydropyrimidine

: 116692-94-5
2-(p-chlorophenyl)-3-phenyl-8,9-bis-(2,2,2-trichloroethoxycarbonyl)-2,8,9-triazabicyclo<3.3.1>nona-3,6-diene

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; ethyl acetate / 19 h / Ambient temperature

2: 1.) molecular sieves 4A, trifluoroacetic acid (TFA) / 1.) CH₂Cl₂, 10 min; 2.) CH₂Cl₂, reflux, 23 h

With 4 A molecular sieve; trifluoroacetic acid; In pyridine; ethyl acetate;
DOI:10.1039/P19880000725

Reference yield:

: 109853-28-3
8,9-bis-(2,2,2-trichloroethoxycarbonyl)-3-phenyl-2-oxa-8,9-diazabicyclo<3.3.1>nona-3,6-diene

: 106-47-8
4-chloro-aniline

: 116692-94-5
2-(p-chlorophenyl)-3-phenyl-8,9-bis-(2,2,2-trichloroethoxycarbonyl)-2,8,9-triazabicyclo<3.3.1>nona-3,6-diene

: 116693-21-1
4-(2,2,2-trichloroethoxycarbonylamino)-2-amino>but-3-enyl phenyl ketone

Guidance literature:: With 4 A molecular sieve; trifluoroacetic acid; Yield given. Multistep reaction; 1.) CH₂Cl₂, 10 min; 2.) CH₂Cl₂, reflux, 23 h;
DOI:10.1039/P19880000725