N-{9-[(2R,3R,4R,5R)-3-(tert-Butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-2-yl]-9H-purin-6-yl}-benzamide

Base Information

Chemical Name:N-{9-[(2R,3R,4R,5R)-3-(tert-Butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-2-yl]-9H-purin-6-yl}-benzamide
CAS No.:87735-31-7
Molecular Formula:C₃₃H₅₁N₅O₆Si₂
Molecular Weight:669.969
Hs Code.:

N-{9-[(2R,3R,4R,5R)-3-(tert-Butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-2-yl]-9H-purin-6-yl}-benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-{9-[(2R,3R,4R,5R)-3-(tert-Butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-2-yl]-9H-purin-6-yl}-benzamide

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Technology Process of N-{9-[(2R,3R,4R,5R)-3-(tert-Butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-2-yl]-9H-purin-6-yl}-benzamide

There total 1 articles about N-{9-[(2R,3R,4R,5R)-3-(tert-Butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-2-yl]-9H-purin-6-yl}-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1191-99-7,75454-45-4
2,3-dihydro-2H-furan

: 81691-32-9
N⁶-benzoyl-2',5'-bis-O-(tert-butyldimethylsilyl)adenosine

: 87735-31-7
N-{9-[(2R,3R,4R,5R)-3-(tert-Butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-2-yl]-9H-purin-6-yl}-benzamide

Guidance literature:: With toluene-4-sulfonic acid; In tetrahydrofuran; Yield given;
DOI:10.1248/cpb.30.376

Reference yield:

: 87735-31-7
N-{9-[(2R,3R,4R,5R)-3-(tert-Butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-2-yl]-9H-purin-6-yl}-benzamide

: 81691-33-0
3'-O-tetrahydrofuranyl-N-benzoyladenosine

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; Yield given;
DOI:10.1248/cpb.30.376

Reference yield:

: 87735-31-7
N-{9-[(2R,3R,4R,5R)-3-(tert-Butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-2-yl]-9H-purin-6-yl}-benzamide

: 81705-86-4
(4-Methoxy-phenyl)-phosphoramidic acid (2R,3S,4R,5R)-5-(6-benzoylamino-purin-9-yl)-4-hydroxy-3-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-2-ylmethyl ester 2-chloro-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: tetra-n-butylammonium fluoride / tetrahydrofuran

With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1248/cpb.30.376