Technology Process of ether silyle du coriolate de methyle
There total 5 articles about ether silyle du coriolate de methyle which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 92 percent / imidazole / dimethylformamide / 0.75 h / Ambient temperature
2: 96 percent / aq. H2SO4 / tetrahydrofuran; H2O / 3 h / Ambient temperature
3: 79 percent / 1.) LiN(SiMe3)2, 2.) HMPT / tetrahydrofuran / 1.) -10 to 0 deg C, 1 h; 2.) -80 deg C, 45 min; -15 deg C, 1 h
With
1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; sulfuric acid; lithium hexamethyldisilazane;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
- Guidance literature:
-
With
lithium hexamethyldisilazane;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
-80 deg C, 1 h, -15 deg C, 1 h;
DOI:10.1016/S0040-4039(00)80387-1
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 84 percent / tetrahydrofuran / 1.5 h / -40 - -15 °C
3: 92 percent / imidazole / dimethylformamide / 0.75 h / Ambient temperature
4: 96 percent / aq. H2SO4 / tetrahydrofuran; H2O / 3 h / Ambient temperature
5: 79 percent / 1.) LiN(SiMe3)2, 2.) HMPT / tetrahydrofuran / 1.) -10 to 0 deg C, 1 h; 2.) -80 deg C, 45 min; -15 deg C, 1 h
With
1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; sulfuric acid; lithium hexamethyldisilazane;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
