methyl S-<<<2-<(benzyloxycarbonyl)-L-alanyloxy>-5-chlorophenyl>methyl>thio>-L-cysteinate hydrochloride

Base Information

Chemical Name:methyl S-<<<2-<(benzyloxycarbonyl)-L-alanyloxy>-5-chlorophenyl>methyl>thio>-L-cysteinate hydrochloride
CAS No.:118143-66-1
Molecular Formula:C₂₂H₂₅ClN₂O₆S₂*ClH
Molecular Weight:549.496
Hs Code.:

Synonyms:

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Chemical Property of methyl S-<<<2-<(benzyloxycarbonyl)-L-alanyloxy>-5-chlorophenyl>methyl>thio>-L-cysteinate hydrochloride

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Technology Process of methyl S-<<<2-<(benzyloxycarbonyl)-L-alanyloxy>-5-chlorophenyl>methyl>thio>-L-cysteinate hydrochloride

There total 6 articles about methyl S-<<<2-<(benzyloxycarbonyl)-L-alanyloxy>-5-chlorophenyl>methyl>thio>-L-cysteinate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 321-14-2
5-chloro-2-hydroxybenzoic acid

: 118143-66-1
methyl S-<<<2-<(benzyloxycarbonyl)-L-alanyloxy>-5-chlorophenyl>methyl>thio>-L-cysteinate hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1: 97 percent / LiAlH₄ / diethyl ether / 0.75 h / Heating

2: 97 percent / pyridine / 2 h / 25 °C

3: 91 percent / sodium hydrogen sulfide / methanol / 2 h / Heating

4: 67 percent / CHCl₃; methanol / 24 h / 25 °C

5: 43 percent / methanol / 1.5 h / 25 °C

6: ethyl acetate / 15 h / -12 °C

With pyridine; sodium hydrogensulfide; lithium aluminium tetrahydride; In methanol; diethyl ether; chloroform; ethyl acetate;
DOI:10.1021/jo00268a020

Reference yield:

: 1142-20-7
N-Cbz-Ala

: 118143-66-1
methyl S-<<<2-<(benzyloxycarbonyl)-L-alanyloxy>-5-chlorophenyl>methyl>thio>-L-cysteinate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / ethyl acetate / -12 °C

2: ethyl acetate / 15 h / -12 °C

With triethylamine; In ethyl acetate;
DOI:10.1021/jo00268a020

Reference yield:

: 6296-67-9
2-acetoxy-5-chlorobenzyl acetate

: 118143-66-1
methyl S-<<<2-<(benzyloxycarbonyl)-L-alanyloxy>-5-chlorophenyl>methyl>thio>-L-cysteinate hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / sodium hydrogen sulfide / methanol / 2 h / Heating

2: 67 percent / CHCl₃; methanol / 24 h / 25 °C

3: 43 percent / methanol / 1.5 h / 25 °C

4: ethyl acetate / 15 h / -12 °C

With sodium hydrogensulfide; In methanol; chloroform; ethyl acetate;
DOI:10.1021/jo00268a020