Methyl (E)-4--3-butenoate

Base Information

Chemical Name:Methyl (E)-4--3-butenoate
CAS No.:72161-40-1
Molecular Formula:C₁₅H₁₆O₄
Molecular Weight:260.29
Hs Code.:

Methyl (E)-4-<o-(2(E)-(methoxycarbonyl)vinyl)-phenyl>-3-butenoate

Synonyms:

Suppliers and Price of Methyl (E)-4--3-butenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl (E)-4--3-butenoate

Chemical Property:

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Technology Process of Methyl (E)-4--3-butenoate

There total 5 articles about Methyl (E)-4--3-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69303-81-7
(R)-3-<(Methoxycarbonyl)methyl>-1,2,3,4-tetrahydroisoquinoline-1-thione

: 72161-40-1
Methyl (E)-4--3-butenoate

Guidance literature:: Multi-step reaction with 4 steps

1: CH₂Cl₂ / 3 h / Ambient temperature

2: Ph₃P,t-BuOK / xylene; 2-methyl-propan-2-ol / 16 h / Heating

3: H₂ / PtO₂ / ethanol / 1 h / Ambient temperature; atmospheric pressure H₂

4: formic acid / 1 h / Heating

With potassium tert-butylate; hydrogen; triphenylphosphine; platinum(IV) oxide; In formic acid; ethanol; dichloromethane; xylene; tert-butyl alcohol;
DOI:10.1021/jo01290a035

Reference yield:

: 66520-42-1
(R)-3-<(Methoxycarbonyl)methyl>-3,4-dihydroisocarbostyril

: 72161-40-1
Methyl (E)-4--3-butenoate

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / P₂S₅ / benzene / 2 h / Heating

2: CH₂Cl₂ / 3 h / Ambient temperature

3: Ph₃P,t-BuOK / xylene; 2-methyl-propan-2-ol / 16 h / Heating

4: H₂ / PtO₂ / ethanol / 1 h / Ambient temperature; atmospheric pressure H₂

5: formic acid / 1 h / Heating

With tetraphosphorus decasulfide; potassium tert-butylate; hydrogen; triphenylphosphine; platinum(IV) oxide; In formic acid; ethanol; dichloromethane; xylene; tert-butyl alcohol; benzene;
DOI:10.1021/jo01290a035

Reference yield:

: 72161-37-6
(R)-3-<(Methoxycarbonyl)methyl>-1-<(methoxycarbonyl)methylidene>-1,2,3,4-tetrahydroisoquinoline

: 72161-40-1
Methyl (E)-4--3-butenoate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / PtO₂ / ethanol / 1 h / Ambient temperature; atmospheric pressure H₂

2: formic acid / 1 h / Heating

With hydrogen; platinum(IV) oxide; In formic acid; ethanol;
DOI:10.1021/jo01290a035