μ2-S-[bis(benzenethiolato)tetranitrosyldiiron]

Base Information

• Chemical Name: μ2-S-[bis(benzenethiolato)tetranitrosyldiiron]
• CAS No.: 1262207-74-8
• Molecular Formula: C₁₂H₁₀Fe₂N₄O₄S₂
• Molecular Weight: 450.062

Synonyms:

Chemical Property of μ2-S-[bis(benzenethiolato)tetranitrosyldiiron]

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of μ2-S-[bis(benzenethiolato)tetranitrosyldiiron]

There total 1 articles about μ2-S-[bis(benzenethiolato)tetranitrosyldiiron] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

Sodium thiosulfate pentahydrate + Na2[Fe2(thiosulfato)2(NO)4]*4H2O + thiophenol (108-98-5) → μ2-S-[bis(benzenethiolato)tetranitrosyldiiron] (20959-77-7,1262207-74-8,1031443-01-2)

Guidance literature:

With NaOH; In water; H2O satd. with Ar for 30 min and added to a mixt. of Na2S2O3*5H2O, Fe complex, NaOH, and C6H5SH; stirred at ca 20°C for 2 h; extd. (CH2Cl2), concd., filtered, crystd. on air for hours, dried in air; elem. anal.;

DOI:10.1007/s11172-010-0215-z

Reference yield:

μ2-S-[bis(benzenethiolato)tetranitrosyldiiron] (20959-77-7,1262207-74-8,1031443-01-2) → nitrogen(II) oxide (10102-43-9)

Guidance literature:

In water; dimethyl sulfoxide; at 25°C under aerobic and anaerobic conditions; not isolated, detected electrochemically; Kinetics;

DOI:10.1007/s11172-010-0215-z

upstream raw materials:

thiophenol

Downstream raw materials:

nitrogen(II) oxide

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