Methyl-onat

Base Information

Chemical Name:Methyl-onat
CAS No.:116302-84-2
Molecular Formula:C₅₈H₆₆O₁₇
Molecular Weight:1035.15
Hs Code.:

Methyl-<methyl-7,8-di-O-acetyl-5-O-(2-acetyl-3,4,6,7-tetra-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-4-O-benzyl-3-desoxy-β-D-manno-2-octulopyranosid>onat

Synonyms:

Suppliers and Price of Methyl-onat

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Methyl-onat

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Methyl-onat

There total 8 articles about Methyl-onat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73650-01-8
methyl (methyl 4,5,7,8-tetra-O-acetyl-3-deoxy-β-D-manno-2-octulopyranosid)onate

: 116302-84-2
Methyl-onat

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) 0.1M CH₃ONa; 2.) imidazole; / 1.) CH₃OH, 2h; 2.) DMF, -10 deg C, 5 min;

2: 1.) dibutylzinnoxide, molecular sieve 4 Angstroem; 2.)tetrabutylammoniumiodide / 1.) toluene, reflux, 2h; 2.) toluene, 40-45 deg C, 8h

3: 1.) silver triflate, molecular sieve 4 Angstroem / 1.) CH₂Cl₂, 1h, 2.) CH₂Cl₂, 48h, -30 deg C - room temp.

4: 1M Bu₄NF / tetrahydrofuran / 15 h

5: 4-(dimethylamino)pyridine / pyridine / 8 h / Ambient temperature

With 1H-imidazole; dmap; 4 A molecular sieve; dibutylzinnoxide; tetrabutyl ammonium fluoride; sodium methylate; silver trifluoromethanesulfonate; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; pyridine;

Reference yield:

: 116302-73-9
Methyl-onat

: 116302-84-2
Methyl-onat

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) dibutylzinnoxide, molecular sieve 4 Angstroem; 2.)tetrabutylammoniumiodide / 1.) toluene, reflux, 2h; 2.) toluene, 40-45 deg C, 8h

2: 1.) silver triflate, molecular sieve 4 Angstroem / 1.) CH₂Cl₂, 1h, 2.) CH₂Cl₂, 48h, -30 deg C - room temp.

3: 1M Bu₄NF / tetrahydrofuran / 15 h

4: 4-(dimethylamino)pyridine / pyridine / 8 h / Ambient temperature

With dmap; 4 A molecular sieve; dibutylzinnoxide; tetrabutyl ammonium fluoride; silver trifluoromethanesulfonate; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; pyridine;

Reference yield:

: 116302-70-6
2-O-Acetyl-3,4,6,7-tetra-O-benzyl-L-glycero-α-D-manno-heptopyranosylchlorid

: 116302-84-2
Methyl-onat

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) silver triflate, molecular sieve 4 Angstroem / 1.) CH₂Cl₂, 1h, 2.) CH₂Cl₂, 48h, -30 deg C - room temp.

2: 1M Bu₄NF / tetrahydrofuran / 15 h

3: 4-(dimethylamino)pyridine / pyridine / 8 h / Ambient temperature

With dmap; 4 A molecular sieve; tetrabutyl ammonium fluoride; silver trifluoromethanesulfonate; In tetrahydrofuran; pyridine;