cis-4,5-dicarbomethoxy-1,2-cyclohexanedione 2-chlorophenylosazone

Base Information

Chemical Name:cis-4,5-dicarbomethoxy-1,2-cyclohexanedione 2-chlorophenylosazone
CAS No.:145159-82-6
Molecular Formula:C₂₂H₂₂Cl₂N₄O₄
Molecular Weight:477.347
Hs Code.:

Synonyms:

Suppliers and Price of cis-4,5-dicarbomethoxy-1,2-cyclohexanedione 2-chlorophenylosazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of cis-4,5-dicarbomethoxy-1,2-cyclohexanedione 2-chlorophenylosazone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of cis-4,5-dicarbomethoxy-1,2-cyclohexanedione 2-chlorophenylosazone

There total 2 articles about cis-4,5-dicarbomethoxy-1,2-cyclohexanedione 2-chlorophenylosazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 624-48-6
dimethyl cis-but-2-ene-1,4-dioate

: 145159-82-6
cis-4,5-dicarbomethoxy-1,2-cyclohexanedione 2-chlorophenylosazone

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / toluene / Heating

2: 1) m-chloroperbenzoic acid / 1) THF, 0 deg C up to r.t., 90 min, 2) EtOH, 0 deg C up to r.t., overnight

With 3-chloro-benzenecarboperoxoic acid; In toluene;
DOI:10.1016/S0040-4020(01)81986-4

Reference yield:

: 145159-81-5
dimethyl 4,5-bis(trimethylsilyloxy)-cis-Δ⁴-tetrahydrophthalate

: 10449-07-7
(2-chlorophenyl)hydrazine

: 145159-82-6
cis-4,5-dicarbomethoxy-1,2-cyclohexanedione 2-chlorophenylosazone

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; Yield given. Multistep reaction; 1) THF, 0 deg C up to r.t., 90 min, 2) EtOH, 0 deg C up to r.t., overnight;
DOI:10.1016/S0040-4020(01)81986-4