2-[2-(3-Chlorophenyl)hydrazinylidene]-3-oxobutanenitrile

Base Information

Chemical Name:2-[2-(3-Chlorophenyl)hydrazinylidene]-3-oxobutanenitrile
CAS No.:28317-60-4
Molecular Formula:C₁₀H₈ClN₃O
Molecular Weight:221.646
Hs Code.:
DSSTox Substance ID:DTXSID00407414

Synonyms:28317-60-4;SCHEMBL3678595;2-[2-(3-Chlorophenyl)hydrazinylidene]-3-oxobutanenitrile;DTXSID00407414

Suppliers and Price of 2-[2-(3-Chlorophenyl)hydrazinylidene]-3-oxobutanenitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[2-(3-Chlorophenyl)hydrazinylidene]-3-oxobutanenitrile

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:221.0355896
Heavy Atom Count:15
Complexity:318

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)C(=NNC1=CC(=CC=C1)Cl)C#N

Technology Process of 2-[2-(3-Chlorophenyl)hydrazinylidene]-3-oxobutanenitrile

There total 1 articles about 2-[2-(3-Chlorophenyl)hydrazinylidene]-3-oxobutanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1118-61-2
3-Aminocrotononitrile

: 108-42-9
3-chloro-aniline

: 28317-60-4
2-(m-chlorophenylhydrazono)-3-oxobutyronitrile

Guidance literature:: 3-chloro-aniline; With hydrogenchloride; sodium nitrite;

3-Aminocrotononitrile; With hydrogenchloride;
DOI:10.3390/molecules21020241

Reference yield: 63.0%

: 28317-60-4
2-(m-chlorophenylhydrazono)-3-oxobutyronitrile

: 105-56-6
ethyl 2-cyanoacetate

: 123534-11-2
1-(3-Chloro-phenyl)-4-methyl-6-oxo-1,6-dihydro-pyridazine-3,5-dicarbonitrile

Guidance literature:: With ammonium acetate; acetic acid; In benzene; for 24h; Heating;
DOI:10.1016/S0040-4020(01)81038-3

Reference yield:

: 28317-60-4
2-(m-chlorophenylhydrazono)-3-oxobutyronitrile

: 123534-21-4
1-(m-chlorophenyl)-1,6-dihydro-6-oxo-4-styrylpyridazin-3,5-dicarbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / ammonium acetate, glacial acetic / benzene / 24 h / Heating

2: 61 percent / ethanol / 0.5 h / Heating

With ammonium acetate; acetic acid; In ethanol; benzene;
DOI:10.1016/S0040-4020(01)81038-3