Technology Process of C29H43NO3Si
There total 1 articles about C29H43NO3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: diisobutylaluminium hydride / hexane; dichloromethane / 5 h / -50 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: 1H-imidazole / dichloromethane / 24 h / 25 °C / Inert atmosphere
With
1H-imidazole; diisobutylaluminium hydride;
In
hexane; dichloromethane;
DOI:10.1021/jo201215c
- Guidance literature:
-
C29H43NO3Si;
With
hydrogenchloride;
In
1,4-dioxane; diethyl ether;
at 25 ℃;
for 4h;
Inert atmosphere;
With
sodium hydroxide;
In
1,4-dioxane; diethyl ether; water;
Inert atmosphere;
DOI:10.1021/jo201215c
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride / 1,4-dioxane; diethyl ether / 4 h / 25 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: pyridine / dichloromethane / 1 h / 25 °C / Inert atmosphere
3.1: hydrogen / dichloromethane / 16 h / 25 °C / 37503.8 Torr / Inert atmosphere
With
pyridine; hydrogenchloride; hydrogen;
In
1,4-dioxane; diethyl ether; dichloromethane;
DOI:10.1021/jo201215c