Silane, chlorodiphenyl[(1E)-2-phenylethenyl]-

Base Information

Chemical Name:Silane, chlorodiphenyl[(1E)-2-phenylethenyl]-
CAS No.:117229-43-3
Molecular Formula:C₂₀H₁₇ClSi
Molecular Weight:320.893
Hs Code.:

Synonyms:

Suppliers and Price of Silane, chlorodiphenyl[(1E)-2-phenylethenyl]-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Silane, chlorodiphenyl[(1E)-2-phenylethenyl]-

Chemical Property:

Purity/Quality:: 98%min ^*data from raw suppliers

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Technology Process of Silane, chlorodiphenyl[(1E)-2-phenylethenyl]-

There total 1 articles about Silane, chlorodiphenyl[(1E)-2-phenylethenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 18419-53-9
vinyldiphenylchlorosilane

: 117229-43-3
trans-Ph₂SiClCH=CHPh

Guidance literature:: [Cl₂(PCy₃)(IMesH₂)Ru(=CHPh)]; In dichloromethane; for 1h; Heating;
DOI:10.1016/j.jorganchem.2005.07.091

Reference yield: 71.0%

: 117229-43-3
trans-Ph₂SiClCH=CHPh

: [dicarbonyl(η5-cyclopentadienyl)iron]trimethylsilane

: 4111-54-0
lithium diisopropyl amide

: {(η5-C5H4SiMe3)Fe(CO)2SiPh2-trans-CH=CHPh}

Guidance literature:: In tetrahydrofuran; (N2); addn. of LDA to a soln. of (η5-C5H5)Fe(CO)2SiMe3 in THF at 0°C; during stirring of the reaction mixt. for 40 min addn. of trans-(Cl)SiPh2CH=CHPh; permitting the soln. to warm to room temp. and addnl. stirring for 30 min;; solvent removal; extn. (CH2Cl2/hexane 40:60); column chromy. (silica gel, CH2Cl2/hexane 20:80 resp.) of the obtained crude material; recrystn. from hexane; elem. anal.;;

Reference yield: 35.0%

: 117229-43-3
trans-Ph₂SiClCH=CHPh

: sodium dicarbonyl(cyclopentadienyl)ferrate

: trans-{(η5-C5H5)Fe(CO)2SiPh2CH=CHPh}

Guidance literature:: In tetrahydrofuran; (N2); stirring of the mixt. for 30 min;; solvent removal; extn. (CH2Cl2/hexane 40:60); column chromy. (silica gel, CH2Cl2/hexane 20:80 resp.) of the obtained crude material; recrystn. from hexane; elem. anal.;;