(Z)-2-aminocinnamonitrile

Base Information

Chemical Name:(Z)-2-aminocinnamonitrile
CAS No.:72119-96-1
Molecular Formula:C₉H₈N₂
Molecular Weight:144.176
Hs Code.:

Synonyms:

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Chemical Property of (Z)-2-aminocinnamonitrile

Chemical Property:

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Technology Process of (Z)-2-aminocinnamonitrile

There total 7 articles about (Z)-2-aminocinnamonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 552-89-6
2-nitro-benzaldehyde

: 72119-96-1
(Z)-2-aminocinnamonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / dimethylformamide / 0.08 h / ice cooling

2: H₂ / 10 percent palladium/charcoal / methyl acetate

With hydrogen; sodium hydride; palladium on activated charcoal; In acetic acid methyl ester; N,N-dimethyl-formamide;
DOI:10.1021/jo01311a044

Reference yield:

: 6140-13-2
(2-acetylphenyl)carbamic acid ethyl ester

: 72119-96-1
(Z)-2-aminocinnamonitrile

Guidance literature:: Multi-step reaction with 5 steps

1: Br₂ / diethyl ether

2: NaBH₄ / tetrahydrofuran

3: 88 percent / NaOH/TBAI / H₂O; CH₂Cl₂ / 0.75 h

4: 64 percent / dimethylformamide / 17 h

5: K₂CO₃ / methanol; H₂O / 10 h / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; bromine; tetra-(n-butyl)ammonium iodide; potassium carbonate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(89)80047-X

Reference yield:

: 122807-12-9
ethyl N-<2-(bromoacetyl)phenyl>carbamate

: 72119-96-1
(Z)-2-aminocinnamonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄ / tetrahydrofuran

2: 88 percent / NaOH/TBAI / H₂O; CH₂Cl₂ / 0.75 h

3: 64 percent / dimethylformamide / 17 h

4: K₂CO₃ / methanol; H₂O / 10 h / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; tetra-(n-butyl)ammonium iodide; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(89)80047-X