Brombis(trimethylsilyl)methan

Base Information

• Chemical Name: Brombis(trimethylsilyl)methan
• CAS No.: 78907-42-3
• Molecular Formula: C₁₅H₂₉BrSSi₃
• Molecular Weight: 405.622
• Mol file: 78907-42-3.mol

Synonyms:

Chemical Property of Brombis(trimethylsilyl)methan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Brombis(trimethylsilyl)methan

There total 3 articles about Brombis(trimethylsilyl)methan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

Brom(bromdimethylsilyl)bis(trimethylsilyl)methan (62139-74-6) + sodium thiophenolate (930-69-8) → Brombis(trimethylsilyl)methan (78907-42-3)

Guidance literature:

In tetrahydrofuran;

Reference yield:

dibromobis(trimethylsilyl)methane (29955-10-0) → Brombis(trimethylsilyl)methan (78907-42-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 95 percent / BuLi / tetrahydrofuran; hexane; diethyl ether / -115 deg C to r.t.

2: 96 percent / Br₂ / 2 h / 60 °C

3: 51 percent / tetrahydrofuran

With n-butyllithium; bromine; In tetrahydrofuran; diethyl ether; hexane;

Reference yield:

Brom(dimethylphenylsilyl)bis(trimethylsilyl)methan (78907-46-7) → Brombis(trimethylsilyl)methan (78907-42-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / Br₂ / 2 h / 60 °C

2: 51 percent / tetrahydrofuran

With bromine; In tetrahydrofuran;

upstream raw materials:

Brom(bromdimethylsilyl)bis(trimethylsilyl)methan

sodium thiophenolate

dibromobis(trimethylsilyl)methane

Brom(dimethylphenylsilyl)bis(trimethylsilyl)methan

Downstream raw materials:

C₁₅H₂₉LiSSi₃

lithium thiophenoxide

1,1,3,3-tetramethyl-2,2,4,4-tetrakis(trimethylsilyl)-1,3-disilacyclobutane

bis(trimethylsilyl)methan