dibenzhydryl O^2'-benzoyl-S-7'-chloro-7'-deoxygriseolate

Base Information

Chemical Name:dibenzhydryl O^2'-benzoyl-S-7'-chloro-7'-deoxygriseolate
CAS No.:98889-99-7
Molecular Formula:C₄₇H₃₆ClN₅O₈
Molecular Weight:834.285
Hs Code.:

dibenzhydryl O<sup>2'</sup>-benzoyl-S-7'-chloro-7'-deoxygriseolate

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Chemical Property of dibenzhydryl O^2'-benzoyl-S-7'-chloro-7'-deoxygriseolate

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Technology Process of dibenzhydryl O^2'-benzoyl-S-7'-chloro-7'-deoxygriseolate

There total 2 articles about dibenzhydryl O^2'-benzoyl-S-7'-chloro-7'-deoxygriseolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.5%

: 98889-87-3
dibenzhydryl O^2'-benzoyl-O^7'-trifluoromathanesulfonylgriseolate

: 98889-99-7,115458-61-2
dibenzhydryl O^2'-benzoyl-S-7'-chloro-7'-deoxygriseolate

Guidance literature:: With lithium chloride; In N,N-dimethyl-formamide; at 100 ℃; for 1h;
DOI:10.1248/cpb.35.4442

Reference yield:

: 98871-19-3
(5R,6R,6aS)-5-(6-Amino-purin-9-yl)-2-((R)-benzhydryloxycarbonyl-hydroxy-methyl)-6-benzoyloxy-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid benzhydryl ester

: 98889-99-7,115458-61-2
dibenzhydryl O^2'-benzoyl-S-7'-chloro-7'-deoxygriseolate

Guidance literature:: Multi-step reaction with 2 steps

1: 79.5 percent / 4-(dimethylamino)pyridine, phosphorous pentoxide / CH₂Cl₂ / 2 h / protection from moisture

2: 69.5 percent / lithium chloride / dimethylformamide / 1 h / 100 °C

With dmap; phosphorus pentaoxide; lithium chloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.35.4442

Reference yield:

: 98889-99-7,115458-61-2
dibenzhydryl O^2'-benzoyl-S-7'-chloro-7'-deoxygriseolate

: 98890-01-8
7'-deoxygriseolic acid

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid, anisole / 0.5 h

2: 20 percent (v/v) ammonia / methanol / 2 h / Ambient temperature

3: 54.6 percent / zinc / acetic acid; H₂O

With ammonia; methoxybenzene; trifluoroacetic acid; zinc; In methanol; water; acetic acid;
DOI:10.1248/cpb.35.4442