1,1,3,3-tetraphenyl-2--4,4-bis(trimethylsilyl)-1,3-disilacyclobutane

Base Information

• Chemical Name: 1,1,3,3-tetraphenyl-2--4,4-bis(trimethylsilyl)-1,3-disilacyclobutane
• CAS No.: 70057-37-3
• Molecular Formula: C₄₀H₅₆Si₆
• Molecular Weight: 705.398

Synonyms:

Chemical Property of 1,1,3,3-tetraphenyl-2--4,4-bis(trimethylsilyl)-1,3-disilacyclobutane

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 1,1,3,3-tetraphenyl-2--4,4-bis(trimethylsilyl)-1,3-disilacyclobutane

There total 5 articles about 1,1,3,3-tetraphenyl-2--4,4-bis(trimethylsilyl)-1,3-disilacyclobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

1,1,2,2-tetraphenyl-3--4,4-bis(trimethylsilyl)-1,2-disilacyclobutane (70057-34-0) + anthracene (120-12-7) → 1,1,3,3-tetraphenyl-2--4,4-bis(trimethylsilyl)-1,3-disilacyclobutane (70057-37-3) + C35H38Si3 (77607-90-0)

Guidance literature:

at 250 ℃; for 3h; sealed tube;

DOI:10.1021/ja00399a031

Reference yield: 26.0%

1,1,2,2-tetraphenyl-3--4,4-bis(trimethylsilyl)-1,2-disilacyclobutane (70057-34-0) → 1,1,3,3-tetraphenyl-2--4,4-bis(trimethylsilyl)-1,3-disilacyclobutane (70057-37-3) + 1,1-dimethyl-2--3,3-diphenyl-4,4-bis(phenyldimethylsilyl)-1,3-disilacyclobutane (77607-89-7)

Guidance literature:

at 250 ℃; for 3h; sealed tube;

DOI:10.1021/ja00399a031

Reference yield:

1,1,2,2-tetraphenyl-3--4,4-bis(trimethylsilyl)-1,2-disilacyclobutane (70057-34-0) → 1,1,3,3-tetraphenyl-2--4,4-bis(trimethylsilyl)-1,3-disilacyclobutane (70057-37-3)

Guidance literature:

at 250 ℃; for 3h;

DOI:10.1021/ja00499a083

upstream raw materials:

1,1,2,2-tetraphenyl-3--4,4-bis(trimethylsilyl)-1,2-disilacyclobutane

methanol

anthracene

1,1,2,2-tetraphenyl-3,4-bis-1,2-disilacyclobutane

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